HomeMy WebLinkAboutStaff Report 6696
City of Palo Alto (ID # 6696)
City Council Staff Report
Report Type: Consent Calendar Meeting Date: 4/4/2016
City of Palo Alto Page 1
Summary Title: Transportation and Disposal of Ash and Sludge
Title: Approval of a Wastewater Treatment Fund Contract With PSC Industrial
Outsourcing, Inc. in a Total Amount Not- to-Exceed $483,703.56 for a Three-
Year Term to Transport and Dispose of Ash and Sludge for the Regional Water
Quality Control Plant
From: City Manager
Lead Department: Public Works
Recommendation
Staff recommends that Council approve and authorize the City Manager or his
designee to execute the attached contract with PSC Industrial Outsourcing, LP
(PSC) for a period of three years not to exceed amount of $483,703.56 for
transportation and disposal of ash and sludge for the Regional Water Quality
Control Plant (Attachment A).
Background
The Regional Water Quality Control Plant (RWQCP) produces approximately two
tons per day of ash from its sewage sludge incinerators. Ash pickups are weekly
and average 11 to 15 tons per pickup. In recent years, annual ash transport and
disposal service has been between 605 to 723 tons. Engineering design of a
Sludge Dewatering and Loadout Facility (Staff Report ID #5295) is nearly complete
with construction of the facility scheduled for completion in summer 2019. This
will allow for the retirement of the incinerators after 47 years of service.
The ash has been managed as a state hazardous waste and placed in a hazardous
waste landfill instead of a standard landfill since 2007. Staff has investigated the
origin of the soluble copper that violates the state (but not federal) hazardous
waste criteria. Staff has not been able to determine the cause of the soluble
copper or any practical treatment modifications. The soluble copper forming in
City of Palo Alto Page 2
the ash during sludge incineration has not impacted the plant’s air or water
discharges. If the soluble copper level drops below state thresholds for hazardous
waste or hazardous waste stabilization during the contract term, the ash will be
directed to an approved landfill at lower cost. During the contract term, it is
expected that soluble copper levels will remain above 40 parts per million and
require disposal as hazardous waste requiring stabilization.
The existing ash hauler is Clean Harbors Environmental Services, Inc. (Clean
Harbors). Clean Harbors has hauled the ash from 2013 to present. Veolia hauled
the plant ash from 2010 to the 2013. PSC hauled and disposed of the plant’s ash
from 2007 to 2010. PSC provided satisfactory service between 2007 and 2010.
Discussion
PSC will dedicate two sealed bins for ash hauling service. PSC will pick up a full bin
of ash once a week and replace it with an empty bin. PSC will transport the ash to
a state hazardous waste treatment facility operated by Waste Management. The
facility is fully permitted to receive hazardous waste. The facility is located west of
I-5 near the unincorporated area of Kettleman City, approximately 186 miles from
the Plant.
The City’s two sewage sludge incinerators have been operating reliably since
1972, without any serious disruption to the incineration process. However, it is
possible that extended incinerator downtime would leave the City without readily
available sludge treatment and disposal alternatives. As a backup to ash disposal,
PSC will provide emergency sludge transport and disposal in the event the plant’s
two sewage sludge incinerators are both inoperative for a period of more than
approximately four days. Like the ash, PSC has proposed disposal of the raw
sludge at the Waste Management Kettleman Hills Facility. East Bay Municipal
Utilities District (EBMUD) in Oakland, California is an alternate sludge disposal
location during emergency situations. EBMUD has the necessary permits as well
as the experience treating raw sludge from other wastewater treatment agencies.
It can treat sludge on a short-term basis during emergencies and digester
maintenance (e.g., for Richmond, California, Central Marin Sanitation Agency, and
others).
Summary of Bid Process
City of Palo Alto Page 3
A request for quotation for the project was posted on the City’s procurement site
and sent to 91 bidders. The bidding period was 31 days. Bids were received from
two qualified contractors on February 23, 2016 as listed on the attached bid
summary (Attachment B). Staff has reviewed all bids submitted. Bids ranged from
a high of $253,336.80 (Clean Harbors) to a low bid of $156,492.79 (PSC). Staff
recommends that the bid of $156,492.79 submitted by PSC be accepted and that
PSC be declared the lowest responsible bidder. PSC provided the lowest bid for
both one-year, two-year and three-year contract terms. Staff checked references
supplied by the contractor for previous work performed and found no significant
complaints. Staff also checked the Contractor's State License Board and found the
contractor has an active license on file.
Bid Name/Number Transportation and Disposal of Ash and
Sludge / RFQ 161852
Proposed Length of Project 1 year with option to extend two additional
years
Number of Bids Mailed to
Contractors
91 notified through PlanetBids
Number of Bids Mailed to
Builder’s Exchanges
0
Number of downloads 7 prospective bidders, (2 of 7 are Builder’s
exchanges)
Total Days to Respond to Bid 31
Pre-Bid Meeting? Yes
Number of Company Attendees at
Pre-Bid Meeting? 2
Number of Bids Received: 2*
Bid Price Range
From a low of $156,492.79 to a high of
$253,336.80 – 1st contract year
From a low of $483,703.56 to a high of
$783,011.45 – all 3 contract years
*Bid summary provided in Attachment B.
Resource Impact
Funds for the first year of the contract have been appropriated in the FY 2016
Wastewater Treatment Enterprise Fund operating budget. Fund for years two and
City of Palo Alto Page 4
three are contingent upon Council approval of the budget for each subsequent
year.
Policy Implications
This recommendation does not represent any change to existing City policies.
Environmental Review
The recommended action is exempt from review under the California
Environmental Quality Act pursuant to CEQA Guidelines Section 15301 (b), which
exempts negligible expansion of an existing use including operation of publicly-
owned sewerage services, structures, facilities, mechanical equipment, or
topographical features.
Attachments:
Attachment A: Contract C16161852 (PDF)
Attachment B: RFQ 161852 Bid Results Summary (PDF)
Attachment A
DocuSign Envelope ID: 448F9D83-A76E-4EF1-9A95-3F616E43347D
CITY OF PALO ALTO CONTRACT NO. C16161852
GENERAL SERVICES AGREEMENT
THIS AGREEMENT made and entered into on the 2nd day of March, 2016, by and
between the CITY OF PALO ALTO, a California chartered municipal corporation
{"CITY"), and PSC INDUSTRIAL OUTSOURCING, LP, a Delaware Limited Liability
Partnership, located at 5151 San Felipe, Ste 1.601:P~ Houston, TX 77056, Telephone
Number: 925-244-1803 ("CONTRACTOR"). In consideration of their mutual covenants,
the parties hereto agree as follows:
1. SERVICES. CONTRACTOR shall provide or furnish the services (the "Services")
described in the Scope of Services, attached at Exhibit A.
2. EXHIBITS. The following exhibits are attached to and made a part of this
Agreement:
t8J "A" -Scope of Services
t8J "A-1" -Lab Data
t8J "A-2" -Ash Bin Cover Diagram
t8J "B" -Schedule of Performance
t8J "C" -Schedule of Fees
t8J "D" -Insurance Requirements
CONTRACT IS NOT COMPLETE UNLESS ALL IND/CA TED EXHIBITS ARE ATTACHED.
3. TERM.
The term of this Agreement is from April 4, 2016 to April 3, 2019 inclusive,
subject to the provisions of Sections Q and V of the General Terms and
Conditions.
4. SCHEDULE OF PERFORMANCE. CONTRACTOR shall complete the Services within
the term of this Agreement in a reasonably prompt and timely manner based
upon the circumstances and direction communicated to CONTRACTOR, and if
applicable, in accordance with the schedule set forth in the Schedule of
Performance, attached at Exhibit B. Time is of the essence in this Agreement.
5. COMPENSATION FOR ORIGINAL TERM. CITY shall pay and CONTRACTOR agrees
to accept as not-to-exceed compensation for the full performance of the
Services and reimbursable expenses, if any:
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r The total maximum lu mp sum compensation-of
OR
dollars($ );
The sum of dollars ($ per hour, not to exceed a total
maximum compensation amount of dollars ($ ); OR
P: A sum calculated in accordance with the fee schedule set forth at Exhibit
C, not to exceed a total maximum compensation amount of four hundred
eighty three thousand seven hundred three dollars and fifty six cents
($483, 703.56).
CONTRACTOR agrees that it can perform the Services for an amount not to
exceed the total maximum compensation set forth above. Any hours worked or
services performed by CONTRACTOR for which payment would result in a total
exceeding the maximum amount of compensation set forth above for
performance of the Services shall be at no cost to CITY.
r CITY has set aside the sum of dollars ($ ) for Additional
Services. CONTRACTOR shall provide Additional Services only by
advanced, written authorization from the City Manager or designee.
CONTRACTOR, at the CITY's request, shall submit a detailed written
proposal including a description of the scope of services, schedule, level
of effort, and CONTRACTOR's proposed maximum compensation,
including reimbursable expense, for such services. Compensation shall
be based on the hourly rates set forth above or in Exhibit C (whichever is
applicable), or if such rates are not applicable, a negotiated lump sum.
CITY shall not authorize and CONTRACTOR shall not perform any
Additional Services for which payment would exceed the amount set
forth above for Additional Services. Payment for Additional Services is
subject to all requirements and restrictions in this Agreement.
6. COMPENSATION DURING ADDITIONAL TERMS.
r CONTRACTOR'S compensation rates for each additional term shall be the
same as the original term; OR
r CONTRACTOR's compensation rates shall be adjusted effective on the
commencement of each Additional Term. The lump sum compensation
amount, hourly rates, or fees, whichever is applicable as set forth in
section 5 above, shall be adjusted by a percentage equal to the change in
the Consumer Price Index for Urban Wage Earners and Clerical Workers
for the San Francisco-Oakland-San Jose area, published by the United
States Department of Labor Statistics (CPI) which is published most
immediately preceding the commencement of the applicable Additional
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Term, wnich shall be comparedwith fhe CPI published most immediately
preceding the commencement date of the then expiring term.
Notwithstanding the foregoing, in no event shall CONTRACTOR's
compensation rates be increased by an amount exceeding five percent of
the rates effective during the immediately preceding term. Any
adjustment to CONTRACTOR's compensation rates shall be reflected in a
written amendment to this Agreement.
7. INVOICING. Send all invoices to CITY, Attention: Project Manager. The Project
Manager is: James Allen, Dept.: Water Quality Control Plant, Telephone: (650)
329-2243. Invoices shall be submitted in arrears for Services performed. Invoices
shall not be submitted more frequently than monthly. Invoices shall provide a
detailed statement of Services performed during the invoice period and are
subject to verification by CITY. CITY shall pay the undisputed amount of invoices
within 30 days of receipt.
GENERAL TERMS AND CONDITIONS
A. ACCEPTANCE. CONTRACTOR accepts and agrees to all terms and conditions of
this Agreement. This Agreement includes and is limited to the terms and
conditions set forth in sections 1 through 6 above, these general terms and
conditions and the attached exhibits.
B. QUALIFICATIONS. CONTRACTOR represents and warrants that it has the
expertise and qualifications to complete the services described in Section 1 of
this Agreement, entitled "SERVICES," and that every individual charged with the
performance of the services under this Agreement has sufficient skill and
experience and is duly licensed or certified, to the extent such licensing or
certification is required by law, to perform the Services. CITY expressly relies on
CONTRACTOR's representations regarding its skills, knowledge, and
certifications. CONTRACTOR shall perform all work in accordance with generally
accepted business practices and performance standards of the industry,
including all federal, state, and local operation and safety regulations.
C. INDEPENDENT CONTRACTOR. It is understood and agreed that in the
performance of this Agreement, CONTRACTOR and any person employed by
CONTRACTOR shall at all times be considered an independent CONTRACTOR and
not an agent or employee of CITY. CONTRACTOR shall be responsible for
employing or engaging all persons necessary to complete the work required
under this Agreement.
D. SUBCONTRACTORS. CONTRACTOR may not use subcontractors to perform any
Services under this Agreement unless CONTRACTOR obtains prior written
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consent of CITY. CONTRACTOR shall be solely responsible for directing the work
of approved subcontractors and for any compensation due to subcontractors.
E. TAXES AND CHARGES. CONTRACTOR shall be responsible for payment of all
taxes, fees, contributions or charges applicable to the conduct of CONTRACTOR's
business.
F. COMPLIANCE WITH LAWS. CONTRACTOR shall in the performance of the
Services comply with all applicable federal, state and local laws, ordinances,
regulations, and orders.
G. PALO ALTO MINIMUM WAGE ORDINANCE. CONTRACTOR shall comply with all
requirements of the Palo Alto Municipal Code Chapter 4.62 (Citywide Minimum
Wage), as it may be amended from time to time. In particular, for any employee
otherwise entitled to the State minimum wage, who performs at least two (2)
hours of work in a calendar week within the geographic boundaries of the City,
CONTRACTOR shall pay such employees no less than the minimum wage set
forth in Palo Alto Municipal Code section 4.62.030 for each hour worked within
the geographic boundaries of the City of Palo Alto. In addition, CONTRACTOR
shall post notices regarding the Palo Alto Minimum Wage Ordinance in
accordance with Palo Alto Municipal Code section 4.62.060.
H. DAMAGE TO PUBLIC OR PRIVATE PROPERTY. CONTRACTOR shall, at its sole
expense, repair in kind, or as the City Manager or designee shall direct, any
damage to public or private property that occurs in connection with
CONTRACTOR's performance of the Services. CITY may decline to approve and
may withhold payment in whole or in part to such extent as may be necessary to
protect CITY from loss because of defective work not remedied or other damage
to the CITY occurring in connection with CONTRACTOR's performance of the
Services. CITY shall submit written documentation in support of such
withholding upon CONTRACTOR's request. When the grounds described above
are removed, payment shall be made for amounts withheld because of them.
I. WARRANTIES. CONTRACTOR expressly warrants that all services provided under
this Agreement shall be performed in a professional and workmanlike manner in
accordance with generally accepted business practices and performance
standards of the industry and the requirements of this Agreement.
CONTRACTOR expressly warrants that all materials, goods and equipment
provided by CONTRACTOR under this Agreement shall be fit for the particular
purpose intended, shall be free from defects, and shall conform to the
requirements of this Agreement. CONTRACTOR agrees to promptly replace or
correct any material or service not in compliance with these warranties,
including incomplete, inaccurate, or defective material or service, at no further
cost to CITY. The warranties set forth in this section shall be in effect for a period
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of one year from completion of tile Services and-shalf survive the completion of
the Services or termination of this Agreement.
J. MONITORING OF SERVICES. CITY may monitor the Services performed under this
Agreement to determine whether CONTRACTOR's work is completed in a
satisfactory manner and complies with the provisions of this Agreement.
K. CITY'S PROPERTY. Any reports, information, data or other material (including
copyright interests) developed, collected, assembled, prepared, or caused to be
prepared under this Agreement will become the property of CITY without
restriction or limitation upon their use and will not be made available to any
individual or organization by CONTRACTOR or its subcontractors, if any, without
the prior written approval of the City Manager.
L. AUDITS. CONTRACTOR agrees to permit CITY and its authorized representatives
to audit, at any reasonable time during the term of this Agreement and for three
(3) years from the date of final payment, CONTRACTOR's records pertaining to
matters covered by this Agreement. CONTRACTOR agrees to maintain accurate
books and records in accordance with generally accepted accounting principles
for at least three (3) following the terms of this Agreement.
M. NO IMPLIED WAIVER. No payment, partial payment, acceptance, or partial
acceptance by CITY shall operate as a waiver on the part of CITY of any of its
rights under this Agreement.
N. INSURANCE. CONTRACTOR, at its sole cost, shall purchase and maintain in full
force during the term of this Agreement, the insurance coverage described at
Exhibit D. Insurance must be provided by companies with a Best's Key Rating of
A-:VII or higher and which are otherwise acceptable to CITY's Risk Manager. The
Risk Manager must approve deductibles and self-insured retentions. In addition,
all policies, endorsements, certificates and/or binders are subject to approval by
the Risk Manager as to form and content. CONTRACTOR shall obtain a policy
endorsement naming the City of Palo Alto as an additional insured under any
general liability or automobile policy. CONTRACTOR shall obtain an
endorsement stating that the insurance is primary coverage and will not be
canceled or materially reduced in coverage or limits until after providing 30 days
prior written notice of the cancellation or modification to the Risk Manager.
CONTRACTOR shall provide certificates of such policies or other evidence of
coverage satisfactory to the Risk Manager, together with the required
endorsements and evidence of payment of premiums, to CITY concurrently with
the execution of this Agreement and shall throughout the term of this
Agreement provide current certificates evidencing the required insurance
coverages and endorsements to the Risk Manager. CONTRACTOR shall include
all subcontractors as insured under its policies or shall obtain and provide to CITY
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separate certificates and endorsements for each subcontractor that meet an the
requirements of this section. The procuring of such required policies of insurance
shall not operate to limit CONTRACTOR's liability or obligation to indemnify CITY
under this Agreement.
0. HOLD HARMLESS. To the fullest extent permitted by law and without limitation
by the provisions of section M relating to insurance, CONTRACTOR shall
indemnify, defend and hold harmless CITY, its Council members, officers,
employees and agents from and against any and all demands, claims, injuries,
losses, or liabilities of any nature, including death or injury to any person,
property damage or any other loss and including without limitation all damages,
penalties, fines and judgments, associated investigation and administrative
expenses and defense costs, including, but not limited to reasonable attorney's
fees, courts costs and costs of alternative dispute resolution), arising out of, or
resulting in any way from or in connection with the performance of this
Agreement. CONTRACTOR's obligations under this Section apply regardless of
whether or not a liability is caused or contributed to by any negligent (passive or
active) act or omission of CITY, except that CONTRACTOR shall not be obligated
to indemnify for liability arising from the sole negligence or willful misconduct of
CITY. The acceptance of the Services by CITY shall not operate as a waiver of the
right of indemnification. The provisions of this Section survive the completion of
the Services or termination of this Agreement.
P. NON-DISCRIMINATION. As set forth in Palo Alto Municipal Code section
2.30.510, CONTRACTOR certifies that in the performance of this Agreement, it
shall not discriminate in the employment of any person because of the race, skin
color, gender, age, religion, disability, national origin, ancestry, sexual
orientation, housing status, marital status, familial status, weight or height of
such person. CONTRACTOR acknowledges that it has read and understands the
provisions of Section 2.30.510 of the Palo Alto Municipal Code relating to
Nondiscrimination Requirements and the penalties for violation thereof, and
agrees to meet all requirements of Section 2.30.510 pertaining to
nondiscrimination in employment.
Q. WORKERS' COMPENSATION. CONTRACTOR, by executing this Agreement,
certifies that it is aware of the provisions of the Labor Code of the State of
California which require every employer to be insured against liability for
workers' compensation or to undertake self-insurance in accordance with the
provisions of that Code, and certifies that it will comply with such provisions, as
applicable, before commencing and during the performance of the Services.
R. TERMINATION. The City Manager may terminate this Agreement without cause
by giving ten (10) days' prior written notice thereof to CONTRACTOR. If
CONTRACTOR fails to perform any of its material obligations under this
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Agreement, in addition to all other remedies provided by law, the City Manager
may terminate this Agreement immediately upon written notice of termination.
Upon receipt of such notice of termination, CONTRACTOR shall immediately
discontinue performance. CITY shall pay CONTRACTOR for services satisfactorily
performed up to the effective date of termination. If the termination if for
cause, CITY may deduct from such payment the amount of actual damage, if any,
sustained by CITY due to CONTRACTOR's failure to perform its material
obligations under this Agreement. Upon termination, CONTRACTOR shall
immediately deliver to the City Manager any and all copies of studies, sketches,
drawings, computations, and other material or products, whether or not
completed, prepared by CONTRACTOR or given to CONTRACTOR, in connection
with this Agreement. Such materials shall become the property of CITY.
S. ASSIGNMENTS/CHANGES. This Agreement binds the parties and their
successors and assigns to all covenants of this Agreement. This Agreement shall
not be assigned or transferred without the prior written consent of CITY. No
amendments, changes or variations of any kind are authorized without the
written consent of CITY.
T. CONFLICT OF INTEREST. In accepting this Agreement, CONTRACTOR covenants
that it presently has no interest, and will not acquire any interest, direct or
indirect, financial or otherwise, which would conflict in any manner or degree
with the performance of this Contract. CONTRACTOR further covenants that, in
the performance of this Contract, it will not employ any person having such an
interest. CONTRACTOR certifies that no CITY Officer, employee, or authorized
representative has any financial interest in the business of CONTRACTOR and
that no person associated with CONTRACTOR has any interest, direct or indirect,
which could conflict with the faithful performance of this Contract.
CONTRACTOR agrees to advise CITY if any conflict arises.
U. GOVERNING LAW. This contract shall be governed and interpreted by the laws
of the State of California.
V. ENTIRE AGREEMENT. This Agreement, including all exhibits, represents the
entire agreement between the parties with respect to the services that may be
the subject of this Agreement. Any variance in the exhibits does not affect the
validity of the Agreement and the Agreement itself controls over any conflicting
provisions in the exhibits. This Agreement supersedes all prior agreements,
representations, statements, negotiations and undertakings whether oral or
written.
W. NON-APPROPRIATION. This Agreement is subject to the fiscal provisions of the
Charter of the City of Palo Alto and the Palo Alto Municipal Code. This
Agreement will terminate without any penalty (a) at the end of any fiscal year in
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thee-vent t hat-fffriosare nor appro·priated for the f6lloWin·g fisca l year, or {orat
any time within a fiscal year in the event that funds are only appropriated for a
portion of the fiscal year and funds for this Contract are no longer available. This
Section shall take precedence in the event of a conflict with any other covenant,
term, condition, or provision of this Contract.
X. ENVIRONMENTALLY PREFERRED PURCHASING AND ZERO WASTE
REQUIREMENTS. CONTRACTOR shall comply with CITY's Environmentally
Preferred Purchasing policies which are available at CITY's Purchasing Division,
which are incorporated by reference and may be amended from time to time.
CONTRACTOR shall comply with waste reduction, reuse, recycling and disposal
requirements of CITY's Zero Waste Program. Zero Waste best practices include
first minimizing and reducing waste; second, reusing waste and third, recycling
or composting waste. In particular, CONTRACTOR shall comply with the
following zero waste requirements:
• All printed materials provided by CONTRACTOR to CITY generated from a
personal computer and printer including but not limited to, proposals,
quotes, invoices, reports, and public education materials, shall be double-
sided and printed on a minimum of 30% or greater post-consumer
content paper, unless otherwise approved by CITY's Project Manager.
Any submitted materials printed by a professional printing company shall
be a minimum of 30% or greater post-consumer material and printed
with vegetable based inks.
• Goods purchased by Contractor on behalf of CITY shall be purchased in
accordance with CITY's Environmental Purchasing Policy including, but
not limited to, Extended Producer Responsibility requirements for
products and packaging. A copy of this policy is on file at the Purchasing
Division's office.
• Reusable/returnable pallets shall be taken back by CONTRCATOR, at no
additional cost to CITY, for reuse or recycling. CONTRACTOR shall provide
documentation from the facility accepting the pallets to verify that pallets
are not being disposed.
V. AUTHORITY. The individual(s) executing this Agreement on behalf of the parties
represent and warrant that they have the legal capacity and authority to do so
on behalf of their respective legal entities.
Z. CONTRACT TERMS: All unchecked boxes do not apply to this Agreement. In the
case of any conflict between the terms of this Agreement and the exhibits hereto
or CONTRACTOR's proposal (if any), the Agreement shall control. In the case of
any conflict between the exhibits hereto and CONTRACTOR's proposal, the
exhibits shall control.
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-AA.DIR REGISTRATION. In regard to any public work construction, alteration,
demolition, repair or maintenance work, CITY will not accept a bid proposal from
or enter into this Agreement with CONTRACTOR without proof that
CONTRACTOR and its listed subcontractors are registered with the California
Department of Industrial Relations ("DIR") to perform public work, subject to
limited exceptions. City requires CONTRACTOR and its listed subcontractors to
comply with the requirements of SB 854.
CITY provides notice to CONTRACTOR of the requirements of California Labor
Code section 1771.l{a), which reads:
"A contractor or subcontractor shall not be qualified to bid on, be listed in a bid
proposal, subject to the requirements of Section 4104 of the Public Contract
Code, or engage in the performance of any contract for public work, as defined
in this chapter, unless currently registered and qualified to perform public work
pursuant to Section 1725.5. It is not a violation of this section for an
unregistered contractor to submit a bid that is authorized by Section 7029.1 of
the Business and Professions Code or Section 10164 or 20103.5 of the Public
Contract Code, provided the contractor is registered to perform public work
pursuant to Section 1725.5 at the time the contract is awarded."
CITY gives notice to CONTRACTOR and its listed subcontractors that
CONTRCATOR is required to post all job site notices prescribed by law or
regulation and CONTRACTOR is subject to SB 854-compliance monitoring and
enforcement by DIR.
CITY requires CONTRACTOR and its listed subcontractors to comply with the
requirements of Labor Code section 1776, including:
Keep accurate payroll records, showing the name, address, social security
number, work classification, straight time and overtime hours worked each day
and week, and the actual per diem wages paid to each journeyman, apprentice,
worker, or other employee employed by, respectively, CONTRACTOR and its
listed subcontractors, in connection with the Project.
The payroll records shall be verified as true and correct and shall be certified and
made available for inspection at all reasonable hours at the principal office of
CONTRACTOR and its listed subcontractors, respectively.
At the request of CITY, acting by its project manager, CONTRACTOR and its listed
subcontractors shall make the certified payroll records available for inspection or
furnished upon request to the project manager within ten (10) days of receipt of
CITY's request.
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-r --CITY requests CONTRACTOR and its listed subcontractors to submit the
certified payroll records to the project manager at the end of each week
during the Project.
If the certified payroll records are not produced to the project manager within
the 10-day period, then CONTRACTOR and its listed subcontractors shall be
subject to a penalty of one hundred dollars ($100.00) per calendar day, or
portion thereof, for each worker, and CITY shall withhold the sum total of
penalties from the progress payment(s) then due and payable to CONTRACTOR.
Inform the project manager of the location of CONTRACTOR's and its listed
subcontractors' payroll records (street address, city and county) at the
commencement of the Project, and also provide notice to the project manager
within five (5) business days of any change of location of those payroll records.
IN WITNESS WHEREOF, the parties hereto have by their duly authorized representatives
executed this Agreement on the date first above written.
CITY OF PALO AL TO
City Manager or Designee
(Required on contracts $85,000 and over)
Title CFO & Treasurer
Telephone: 713-985-5409
Approved as to form:
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1.1 BACKGROUND
EXHIBIT A
SCOPE OF SERVICES
A. The Palo Alto Regional Water Quality Control Plant (RWQCP) operates a sewage sludge incinerator,
which creates a dry ash in the bottom of the furnace. The sludge is thermally transformed into ash
containing inorganic oxides.
B. CONTRACTOR will dispose of the ash at the Waste Management Kettleman Hills Facility (KHF).
C. Vendor has visually observed the bin drop off and pickup site and verified that the hauler's equipment
can safely operate at owner's site.
D. This is a contract for the combined services of hauling and disposal of sludge and ash.
CONTRACTOR is a qualified, licensed hauler with the appropriate contract with a Class 1-nonRCRA
sanitary landfill.
1.2 PURPOSE
A. This contract is for hauling and disposal of ash. The contractor is to maintain qualifications and
licenses to haul the ash to a Class 1-nonRCRA sanitary landfill.
B. The contractor shall transport and dispose of the ash in accordance with the terms and conditions of
this contract. The Contractor shall be expressly designated by the Parties hereto as the transporter of,
and the arranger for the disposal of all wastes to be transported, managed and disposed of under this
contract.
C. The sewage sludge incinerators have been operating since 1972 and producing ash. Though the
incinerators have never failed, the potential exists for incinerator nonoperation and loss of all surplus
sludge storage capacity. In this case, a backup transportation and disposal contract is needed to handle
dewatered, untreated sludge and disposal at a sanitary landfill or at another sewage treatment plant.
1.3 CHARACTERISTICS OF ASH AND SLUDGE
Ash pickups are weekly and average 10 to 13 tons per pickup. A larger load (e.g., 20 tons) is not frequent
and typically occurs after very large storms when the plant is processing a higher solids loading. In most
years, there are 53 ash pickups (historically, they are always on Tuesday mornings). Pickups are
occasionally (once or twice per year) more often than once a week and the CONTRACTOR will respond to
calls for special pickups. Once a year, an industrial cleaning company (not part of this contract) cleans out
one of the plant's incinerators of its ash for special inspection; an extra bin will be requested from the
CONTRACTOR at least once a year for this purpose and drop off shall be within 48 hours. The special
pickup shall not involve one of the two bins used for regular service. Previous year data is shown below, in
tons.
DocuSign Envelope ID: 448F9083-A76E-4EF1-9A95-3F616E43347D
Ye_a_r No. of Loads Totar Minimum 25%ile 50%ile 75%ile Maximum
2010 53 713 11.9 13.1 13.7 14.2 17.9
2011 54 723 10.0 12.6 13.4 14.0 18.0
2012 53 638 7.4 11.2 12.4 13.1 20.2
2013 55 628 2.9 10.7 11.2 12.5 16.8
2014 53 605 5.1 10.3 11.3 12.5 18.8
2015 51 631 6.2 11.3 12.3 14.5 15.7
A. Ash Copper Levels
I. Since about 2007, the plant's ash has been hauled and disposed of as a state hazardous waste
because the soluble copper level exceeded state limits (not federal limits). If the soluble copper
level drops below 25 ppm per state regulations during the contract term, the ash shall be directed
to an approved municipal landfill.
2. Since mid-2011, the soluble copper level in the ash has been over 40 ppm. When the soluble
copper level in the ash is greater than 40 ppm, final disposal will require that the ash be disposed
of in a Class 1 non-RCRA hazardous waste landfill and stabilized prior to disposal, if required by
the jurisdiction of the landfill. If the copper level drops per state requirements below 40 ppm
during the contract term and remains over 25 ppm, the ash shall be direct landfilled at a Class 1
non-RCRA hazardous waste landfill.
3. Unless notified otherwise, the CONTRACTOR shall assume that the soluble copper level remains
greater than 40 ppm during the contract term.
B. In previous years, offloading ash for stabilization, solidification, and disposal was delayed due to dust
control and landfill equipment reliability issues. CONTRACTOR is aware that the material to be
disposed of can easily become airborne and produce dust during treatment and/or offloading;
CONTRACTOR has coordinated with KHF regarding these issues.
C. Wet sludge production is estimated to be 75 tons per day of 28% dry sludge cake (undigested and
untreated).
D. For waste characterization, ash sample lab analysis is included in Exhibit A-1.
1.4 ASH PACKAGING AND TRANSPORTATION
A. The City will load the ash into a bin owned by the contractor and left at the plant site. The contractor
shall provide two watertight, open-top, tarped bins for ash. One bin shall remain at the RWQCP and
the other shall be used by the contractor for exchanges. The contractor shall deliver the bin to the
RWQCP for the temporary storage of the ash. The City will place the ash into the bin and will notify
the contractor for exchange of bin and disposal of the ash when the bin is sufficiently full and ready
for disposal. The bin, each approximately 40 cubic yards, shall be water tight, lined, tarped, and
suitable for transportation of the ash.
B. The City will notify the contractor two calendar days before the required disposal of the ash and bin
exchange. Typical pickups are on Tuesdays. For City holidays falling upon a Tuesday or for other
special coordination, the CONTRACTOR is to work with plant staff to determine an alternate pickup
day. Upon notice, the contractor shall at its expense, remove, transport, and dispose of the ash at an
approved, class 1-nonRCRA sanitary landfill site suitable for proper disposal of ash. Removal and
exchange of the bins shall be between the hours of 6:05 a.m. and 5:30 p.m., upon City notification.
Transportation shall be by licensed, registered hauler who complies with all local, state, and federal
laws.
DocuSign Envelope ID: 448F9D83-A76E-4EF1-9A95-3F616E43347D
C. The City owns and maintains an ash bin cover with a screw to move ash throughout the bin for even
distribution. The waste hauler shall only provide bins compatible with the existing cover. A diagram
and dimensions of the City's ash bin cover is included in Exbibit A-2. The City will remove the ash
bin cover prior to bin pickup.
1.5 EMERGENCY SLUDGE PACKAGING AND TRANSPORTATION
A. The City will load the sludge into a bin owned by the contractor and left at the plant site after
notification of need for this service. The contractor shall provide multiple watertight bins for sludge.
One bin shall remain at the RWQCP and the others shall be used by the contractor for exchanges. The
contractor shall deliver the bin to the RWQCP for the temporary storage of the sludge. The City will
place the sludge into the bin and will notify the contractor for exchange of bin and disposal of the
sludge when the bin is sufficiently full and ready for disposal. The bin, each approximately 20 cubic
yards, shall be water tight, lined, and suitable for transportation of untreated sludge.
B. If the emergency sludge disposal is needed, the hauler will need to mobilize to provide service within
24 hours. The plant will need the change out of five or more CONTRACTOR-supplied 20-cubic yard
drop-off bins per day, 24 hours per day, seven days per week. The hauling and transport of sewage
sludge will continue until the sewage sludge incinerators are repaired. The CONTRACTOR will need
to have made arrangements in advance for this service should it be required.
C. The City will notify the contractor in the event of an emergency need to use their services for sludge
hauling. The contractor shall provide a 24-hour emergency dispatch number. Upon notice, the
contractor shall at its expense, remove, transport, and dispose of the sludge at an approved sanitary
landfill site suitable for proper disposal of untreated sewage sludge. Removal and exchange of the bins
shall be at all hours of plant operation. Temporary storage of sludge bins is available onsite when
landfills are closed. Transportation shall be by licensed, registered hauler who complies with all local,
state, and federal laws.
1.6 WEIGHTS AND ASSAYS
A. The City will keep a record of the estimated weight or volume of each truck load of waste. At its
expense, the contractor shall weigh each truckload of waste received at its disposal site and submit the
weight tags to the RWQCP.
1.7 DOCUMENTATION, PERMITS AND INSURANCE
A. The contractor shall maintain permits and insurance required during the term of this contract.
B. Contractor shall provide all appropriate documentation, certifications and records for the
transportation, management and disposal of Class 1 wastes and all applicable federal, state and local
laws and regulations, including, but not limited to:
1. bills of lading or non-hazardous waste manifests
2. Class I waste manifests and continuation sheets
3. labpack inventory sheets
4. land disposal restriction notifications
5. Class I waste profiles
6. certificates of destruction, decontamination, disposal and/or recycling
Appropriate copies of the documentation listed above as well as any other documents required by the
City's Project Manager shall be furnished to the City's Project Manager at the time of waste shipment.
C. Closed originals of all uniform hazardous (and non-hazardous) waste manifests signed by a duly
authorized representative of the receiving Treatment/Storage/Disposal Facility (TSDF) shall be
DocuSign Envelope ID: 448F9D83-A76E-4EF1-9A95-3F616E43347D
furnished to the City's Project Manager within thirfy (30) calendar days of waste shipment. This
requirement shall survive the expiration and/or termination of the Agreement.
D. Certificates of destruction, decontamination, disposal and/or recycling signed by a duly authorized
representative of the receiving TSDF shall be furnished by the Contractor to the City's Project
Manager for all wastes to be managed under this contract within one hundred and eighty (180)
calendar days of waste shipment. This requirement shall survive the expiration and/or termination of
the Agreement.
E. The Contractor shall, at all times during the transportation, storage, and disposal of wastes to be
managed under this contract, know the location, condition and status of each item being managed. The
Contractor shall make such information available in written progress reports to the City's Project
Manager upon request. The progress reports shall include a listing of items removed, referenced by an
appropriate identification number and uniform Class I waste manifest number and a description of the
location and status of wastes on date of the written progress report.
1.8 PICKUP ADDRESS
A. Palo Alto Regional Water Quality Control Plant
Attn: Operations Shift Supervisor or Senior Operator
2501 Embarcadero Way
Palo Alto, CA 94303
650-329-2598 -phone
1.9 BILLING ADDRESS
B. Palo Alto Regional Water Quality Control Plant
Attn: Mary Sekator
2501 Embarcadero Way
Palo Alto, CA 94303
650-329-2396 -phone
650-494-8395 -fax
1.10 PRICING CONDITIONS AND ANNUAL INCREASES
A. ADDITIONAL PRICING CONDITIONS
1. Demurrage will not be charged for pickup of waste up to and including 90 minutes of loading and
unloading time. After 90 minutes, the demurrage charge of $95/hour applies will apply if the City
causes the delay.
2. Demurrage will not be charged for delays caused by the hauler not having proper paperwork at the
time of arrival at the plant site.
3. Unloading demurrage will not be charged for wastes being delivered unless the City of Palo Alto
creates a condition such as an improperly identified waste or nonconforming waste.
4. A minimum volume of 10 tons (or yards, whichever is greater) will be billed for all waste received
in a roll-off container, intermodal, or dump trailer delivered to hauler's waste disposal facility.
5. Haulers' owned or leased roll-off containers or other equipment that are damaged by City of Palo
Alto may be repaired by contractor and invoice City at a quoted hourly rate for labor and parts
invoiced at no more than cost plus 30%.
6. Roll-off washout charges are to be included in the pricing.
7. In the event sludge can be hauled to East Bay Municipal Utilities District, the pncmg for
emergency sludge disposal shall be cost plus 10%. For the base contract, the prices in Section B
above shall apply.
8. In case of price increase due to new regulatory fees, waste hauler must notify the City of Palo Alto
DocuSign Envelope ID: 448F9D83-A76E-4EF1-9A95-3F616E43347D
ic,-wd[ing before any aclaitional fees will be allowed.
B. ANNUAL INCREASES
1. The price increase for the second and third 12-month periods of this contract is to be determined in
the Base Bid Schedules.
2. In the case of a price increase due to new regulatory fees, the contractor must notify the City of
Palo Alto in writing before any additional fees will be allowed.
1.11 MISCELLANEOUS CONDITIONS
A The waste hauler will have free and easy access to the pickup site.
B. The waste hauler will maintain containers in DOT shippable condition.
C. Composition of Waste
i. If CITY'S waste materials do not conform to the descriptions and specifications in the
corresponding Profile Sheet, CONTRACTOR and CITY shall, in good faith, attempt to amend the
Profile Sheet and any other pertinent documents and/or correct any improper containerization,
marking or labeling to enable CONTRACTOR to accept such non-conforming waste materials at a
Facility. If the parties cannot, within a reasonable time after CONTRACTOR notifies CITY the
waste materials are non-conforming, resolve the same as set forth above, CITY shall make prompt
arrangements for the removal of such non-conforming waste materials from the Facility at which
they are located to another lawful place of storage or disposal. CITY agrees to pay
CONTRACTOR its reasonable expenses and charges incurred with respect to CITY'S' non-
conforming waste materials.
ii. CONTRACTOR ADDITIONAL WARRANTIES CONTRACTOR represents and warrants to
CITY that: a. CONTRACTOR is engaged in the business of performing Services with respect to
waste materials and has developed the requisite expertise to perform the Services agreed to by
CITY and CONTRACTOR hereunder; b. all CONTRACTOR vehicles and each Facility utilized
to perform Services hereunder shall have all permits, licenses, certificates or approvals required
under applicable laws and regulations for such Services; and c. CONTRACTOR will perform
Services for CITY in a safe and workmanlike manner, and in compliance with all statutes,
ordinances, laws, orders, rules and regulations applicable to the Services.
iii. CITY'S WARRANTIES CITY represents and warrants to CONTRACTOR that: a. the
description of and specifications pertaining to its waste materials in the Profile Sheet is and at all
times will be true and correct in all material respects, and waste materials tendered to
CONTRACTOR will at all times, including, without limitation, at the time ofrecertification of the
waste materials, conform to the description and specifications contained in the Profile Sheet; b.
CITY has made available all information it has regarding the waste materials, and if CITY
receives information that the waste materials described in a Profile Sheet present, or may present,
a hazard or risk to persons or the environment not reasonably disclosed in the Profile Sheet, CITY
will promptly report such information to CONTRACTOR; c. if CITY is not the Generator of the
waste materials (as defined in 40 CFR 260.10), CITY has all necessary authority to enter into this
Agreement with respect to the waste materials; d. CITY is under no legal restraint which prohibits
the transfer of possession of such waste materials to CONTRACTOR; e. CITY shall comply with
all applicable statutes, ordinances, laws, orders, rules and regulations, and shall provide
CONTRACTOR a safe work environment for Services performed on any premises owned or
controlled by CITY; and f. if CONTRACTOR requests that work areas be secured, CITY will be
solely responsible for securing such work areas and for preventing anyone other than
CONTRACTOR personnel from entering the designated work areas.
D. TRANSFER OF TITLE CONTRACTOR shall take title to CITY's waste materials which conform to
DocuSign Envelope ID: 448F9D83-A76E-4EF1 -9A95-3F616E43347D
lhc descriptions a11d specifications stated in the Profi le Sheet upon cofr1pletio-n of loadfng info
CONTRACTOR's transportation vehicles, or if transported by CITY, upon acceptance at the Facility.
E. CONTRACTOR acknowledges that a major construction project to construct a sludge dewatering
building will occur in the field south of the ash bin during the contract term. The field south of the bin
will not be available during much of the contract term for maneuvering the hauler's truck. The
construction contractor may move the ash hauler's bin during the construction contract for logistical
purposes. The CONTRACTOR is required to have a reciprocal agreement with the city's construction
contractor allowing free movement of the hauler's bin at no cost to the city or the construction
contractor. The agreement shall cover necessary coordination requirements (e.g., liability for bin
damage). The construction contractor has not been selected. The city's project manager will notify
PSC when the construction contractor has been selected.
F. The City does not expressly or by implication agree that the actual amount of work shall correspond to
approximately weekly pickups in the range of 605 to 723 dry tons/year of ash mentioned in the bid, but
reserves the right to increase, decrease or modify the amount of any class or portion of the work or to
omit portions of the work as may be deemed necessary or expedient by the City's Project Manager.
END OF SECTION
DocuSign Envelope ID: 448F9D83-A76E-4EF1-9A95-3F616E43347D
NELAP/ORELAP Certification 4036 ~ Caltest CA-ELAP Certification 1664
'ANAl\"ll('AI I \llt>ltAlllll\'
Thursday, June 18, 2015
Samantha Bialorucki
City of Palo Alto
2501 Embarcadero Way
Palo Alto, CA 94303
Re Lab Order: 0050123
ENVIRO NMENT -,. A '
Project ID: NP DES QUARTERLY MAY 2015
Dear Samantha Bialorucki:
I, ' S
EXHIBIT A-1
Lab Data
Collected By: WQCP LAB AND OPS
PO/Contract#: 4615000068
Enclosed are the analytical results for sample(s) received by the laboratory on Tuesday, May 05, 2015. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Enclosures
Project Manager: Melinda F. Kelley
6/18/2015 16:12 REPORT OF LABORATORY ANALYSIS Page 1 of 27
This report shall not be reproduced, except In full,
without the written consent of CAL TEST ANALYTICAL LABORATORY
1885 North Kelly Road• Napa, California 94558
(707) 258-4000 • Fax (707) 226-1001 • e-mail: info@caltestlabs.com
DocuSign Envelope ID: 448F9D83-A76E-4EF1-9A95-3F616E43347D
NELAP/ORELAP Certification 4036 ~~~ Caltest ~-~ -~~~~ • t(~i .\N/\1 \ l lC\I. I \II< Ill\ I OH\
SAMPLE SUMMARY
Lab Order: Q050123
Project ID: NPDES QUARTERLY MAY 2015
Lab ID Sample ID Matrix
Q050123001 E000764-01 ASH A
Q050123002 E000763-01 ASH A
Q050123003 E000765-01 ASH A
Q050123004 E000766·01 BARSCREEN RAGS
Solid
Solid
Solid
Solid
Solid Q050123005 E000767-01 GRIT
6/18/2015 16:12 REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of CALTEST ANALYTICAL LABORATORY
1885 North Kelly Road• Napa, California 94558
CA-ELAP Certification 1664
011
Date Collected Date Received
05/04/2015 10:00 05/05/2015 13:40
05/04/2015 10:00 05/05/2015 13:40
05/04/2015 10:00 05/05/2015 13:40
05/04/2015 09:33 05/05/2015 13:40
05/04/2015 09:35 05/05/2015 13:40
Page 2 of 27
(707) 258-4000 • Fax (707) 226-1001 • e-mail: info@caltestlabs.com
DocuSign Envelope ID: 448F9083-A76E-4EF1-9A95-3F616E433470
NELAP/ORELAP Certification 4036 CA-ELAP Certification 1664
II REVLSED II
NARRATIVE
Lab Order: 0050123
Project ID: NPDES QUARTERLY MAY 2015
General Quallflers and Notes
Caltest authorizes this report to be reproduced only in its entirety. Results are specific to the sample(s) as submitted and only to
the parameter(s) reported.
Caltest certifies that all test results for wastewater and hazardous waste analyses meet all applicable NELAC requirements; all
microbiology and drinking water testing meet applicable ELAP requirements, unless stated otherwise.
All analyses performed by EPA Methods or Standard Methods (SM) 20th Edition except where noted (SMOL=online edition).
Caltest collects samples in compliance with 40 CFR, EPA Methods, Cal. Title 22, and Standard Methods.
Dilution Factors (OF) reported greater than '1' have been used to adjust the result, Reporting Limit (RL), and Method Detection
Limit (MDL).
All Solid, sludge, and/or biosolids data is reported in Wet Weight, unless otherwise specified.
Filtrations performed at Caltest for dissolved metals (excluding mercury) and/or pH analysis are not performed within the 15
minute holding time as specified by 40CFR 136.3 table II.
Results Qualifiers: Report fields may contain codes and non-numeric data correlating to one or more of the following definitions:
ND -Non Detect -indicates analytical result has not been detected.
RL -Reporting Limit Is the quantitation limit at which the laboratory Is able to detect an analyte. An analyte not detected at or
above the RL is reported as ND unless otherwise noted or qualified. For analyses pertaining to the State Implementation Plan of
the California Toxics Rule, the Caltest Reporting Limit (RL) is equivalent to the Minimum Level (ML). A standard is always run at or
below the ML. Where Reporting Limits are elevated due to dilution, the ML calibration criteria has been met.
J -reflects estimated analytical result value detected below the Reporting Limit (RL) and above the Method Detection Limit (MDL).
The 'J' flag is equivalent to the ONO Estimated Concentration flag.
E -indicates an estimated analytical result value.
B -indicates the analyte has been detected in the blank associated with the sample.
NC -means not able to be calculated for RPO or Spike Recoveries.
SS -compound is a Surrogate Spike used per laboratory quality assurance manual.
NOTE: This document represents a complete Analytical Report for the samples referenced herein and should be retained as a
permanent record thereof.
Workorder Notes
Report revised to reflect current MDLs for 60108 (Leachate)
Qualifiers and Compound Notes
2
3
4
5
6
6/18/2015 16:12
Analyte(s) reported as 'ND' means not detected at or above the listed Method Detection Limits (MDL).
The Reporting Limit (R.L.) was raised due to background interference noted in the sample.
Sample diluted due to a high concentration of non-target analyte(s), resulting in increased reporting limits.
Initial sample amount reduced in prep in an effort to reduce matrix effects resulting in higher reporting limit(s).
Sample diluted to bring concentration of target analyte(s) within the working range of the instrument, resulting in
increased reporting limits.
Sample prepared using methanolic extraction method resulting In higher reporting limit(s).
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of CAL TEST ANALYTICAL LABORATORY
1885 North Kelly Road• Napa, California 94558
(707) 258-4000 • Fax (707) 226-1001 • e-mail: info@caltestlabs.com
Page 3 of 27
ATTACHMENT A
DocuSign Envelope ID: 448F9D83-A76E-4EF1-9A95-3F616E43347D
NELAP/ORELAP Certification 4036 ;,r~
'~ Caltest
' ,\N,\IYl'l<'/\1. L\IIDIIATOIIV
CA-ELAP Certification 1664
ENVIRONMENTAL ANALYSES
ANALYTICAL RESULTS
Lab Order: 0050123
Project ID: NPDES QUARTERLY MAY 2015
Solid results are reported on a wet weight basis.
Lab ID Q050123001 Date Collected 5/4/2015 10:00 Matrix Solid
Sample ID E000764-01 ASH A Date Received 5/5/2015 13:40 Results are expressed as wet weight values
Parameters Result Units R. L. MDL DF Prepared Batch Analyzed Batch Qua I
Mercury Analysis Prep Method: SW846 7471A Prep by: UK
Analytical Method: SW846 7471A Analyzed by: LM
Mercury J0.0009 mg/kg 0.020 0.00080 1 05/06/15 00:00 MPR 13565 05/07/15 13:12 MHG 4963
Metals Analysls by ICP Prep Method: SW846 30508 Prep by: UK
Analytical Method: SW846 60108 Analyzed by: LM
Antimony 3.5 mg/kg 2.0 1.5 1 05/06/15 00:00 MPR 13563 05/18/15 00:00 MIC4479
Arsenic 4.6 mg/kg 2.0 1.0 1 05/06/15 00:00 MPR 13563 05/11/15 00:00 MIC 4479
Barium 830 mg/kg 1.0 0.70 1 05/06/15 00:00 MPR 13563 05/11/15 00:00 MIC4479
Beryllium ND mg/kg 5.0 0.15 1 05/06/15 00:00 MPR 13563 05/11/15 00:00 MIC4479 2,1
Cadmium 0.36 mg/kg 0.20 0.050 1 05/06/15 00:00 MPR 13563 05/11 /15 00:00 MIC4479
Chromium 70 mg/kg 1.0 0.20 1 05/06/15 00:00 MPR 13563 05/11 /15 00:00 MIC4479
Cobalt 19 mg/kg 0.4 0.20 1 05/06/15 00:00 MPR 13563 05/11/15 00:00 MIC4479
Copper 1900 mg/kg 4.0 0.40 2 05/06/15 00:00 MPR 13563 05/14/15 00:00 MIC4479
Lead 55 mg/kg 1.0 0.50 1 05/06/15 00:00 MPR 13563 05/11 /15 00:00 MIC 4479
Molybdenum 29 mg/kg 2.0 1.0 1 05/06/15 00:00 MPR 13563 05/11 /15 00:00 MIC 4479
Nickel 81 mg/kg 1.0 0.30 1 05/06/15 00:00 MPR 13563 05/11/15 00:00 MIC 4479
Selenium 7.9 mg/kg 2.0 0.80 1 05/06/15 00:00 MPR 13563 05/11/15 00:00 MIC4479
Silver 14 mg/kg 1.0 0.15 1 05/06/15 00:00 MPR 13563 05/11/15 00:00 MIC 4479
Thallium 2.6 mg/kg 2.0 0.70 1 05/06/15 00:00 MPR 13563 05/11/15 00:00 MIC4479
Vanadium 77 mg/kg 0.40 0.20 1 05/06/15 00:00 MPR 13563 05/11/15 00:00 MIC4479
Zinc 2000 mg/kg 8.0 2.0 2 05/06/15 00:00 MPR 13563 05/14/15 00:00 MIC 4479
Cyanide, Total Analysls Analytical Method: SW846 9012A Analyzed by: BCP
Cyanide 0.69 mg/kg 0.080 0.080 05/09/15 17:05 wco 10778
Percent Sollds Analysls Analytlcal Method: SM20-2540 G Analyzed by: JDC
Solids, Percent 100 % 0.1 0.1 05/07/15 17:04 WGR5763
Lab ID Q050123002 Date Collected 5/4/2015 10:00 Matrix Solid
Sample ID E000763-01 ASH A Date Received 5/5/2015 13:40 Results are expressed as wet weight values
Parameters Result Units R. L. MDL DF Prepared Batch Analyzed Batch Qua I
Mercury Analysis, STLC Prep Method: SW846 7470A Prep by: UK
Analytlcal Method: SW846 7470A Analyzed by: LM
Mercury ND ug/L 0.50 0.30 105/12/1500:00 MPR 13577 05/13/15 13:51 MHG 4968
Metals Analysis by ICP, STLC Prep Method: SW846 3010 Prep by: UK
Analytical Method: SW846 60108 (Leachate) Analyzed by: LM
Barium 16 mg/L 0.15 0.070 1 05/11 /15 00:00 MPR 13573 05/14/15 00:00 MIC 4481
Copper 40 mg/L 0.10 0.030 1 05/11 /15 00:00 MPR 13573 05/14/15 00:00 MIC 4481
Lead 0.19 mg/L 0.10 0.040 1 05/11 /15 00:00 MPR 13573 05/14/15 00:00 MIC 4481
Silver ND mg/L 0.030 0.0060 1 05/11/15 00:00 MPR 13573 05/14/15 00:00 MIC 4481
6/18/2015 16:12 REPORT OF LABORATORY ANALYSIS Page 4 of 27
This report shall not be reproduced, except in full,
without the written consent of CAL TEST ANALYTICAL LABORATORY
1885 North Kelly Road• Napa, California 94558
(707) 258-4000 • Fax (707) 226-1001 • e-mail: info@caltestlabs.com
DocuSign Envelope ID: 448F9D83-A76E-4EF1-9A95-3F616E43347D
NELAP/ORELAP Certification 4036 ·,~, Caltest
,·~ ,\~AlnlC.\I I \l!tll:\IOHY
CA-ELAP Certification 1664
II REVISED II
ANALYTICAL RESULTS
Lab Order: 0050123
Project ID: NPDES QUARTERLY MAY 2015
Solid results are reported on a wet weight basis.
Lab ID Q050123003 Date Collected 5/4/2015 10:00 Matrix Solid
Sample ID E000765-01 ASH A Date Received 5/5/2015 13:40 Results are expressed as wet weight values
Parameters Result Units R. L. MDL DF Prepared Batch Analyzed Batch Qual
~~~~~-~~~~~-~~~~~~~~~
Asbestos Analysis -Solid Analytical Method: (per attached report) Asbestos Analysis· Solld
Analysis performed by EMSL Analytical, CA-ELAP Certification 1620. Refer to attached for original certificate of analysis.
Lab ID Q050123004 Date Collected 5/4/2015 09:33 Matrix Solid
Sample ID E000766-01 BARSCREEN Date Received 5/5/2015 13:40 Results are expressed as wet weight values
RAGS
Parameters Result Units R. L. MDL DF Prepared Batch Analyzed Batch Qua I
Mercury Analysis, STLC, Low Level Prep Method: SW846 7 4 70A Low Level Prep by: UK
Analytical Method: SW846 7 4 70A Low Level Analyzed by: LM
Mercury ND ug/L 0.50 0.30 1 05/12/15 00:00 MPR 13577 05/13/15 13:54 MHG 4968
Mercury Analysis Prep Method: SW846 7471A Prep by: UK
Analytical Method: SW846 7471A Analyzed by: LM
Mercury 0.032 mg/kg 0.020 0.00079 1 05/06/15 00:00 MPR 13565 05/07 /15 13:44 MHG 4963
Metals Analysis by ICP, STLC Prep Method: SW846 3010 Prep by: UK
Analytical Method: SW846 60108 (Leachate) Analyzed by: LM
Antimony ND mg/L 0.10 0.040 1 05/11/15 00:00 MPR 13573 05/14/15 00:00 MIC 4481
Arsenic 0.34 mg/L 0.10 0.050 1 05/11 /15 00:00 MPR 13573 05/14/15 00:00 MIC 4481
Barium 0.45 mg/L 0.15 0.070 1 05/11 /15 00:00 MPR 13573 05/14/15 00:00 MIC4481
Beryllium ND mg/L 0.010 0.0050 105/11/1500:00 MPR 13573 05/14/15 00:00 MIC 4481
Cadmium ND mg/L 0.010 0.0040 105/11/1500:00 MPR 13573 05/14/15 00:00 MIC 4481
Chromium ND mg/L 0.10 0.050 1 05/11/15 00:00 MPR 13573 05/14/15 00:00 MIC 4481
Cobalt ND mg/L 0.050 0.020 1 05/11/15 00:00 MPR 13573 05/14/15 00:00 MIC 4481
Copper ND mg/L 0.10 0.030 1 05/11/15 00:00 MPR 13573 05/14/15 00:00 MIC 4481
Lead ND mg/L 0.10 0.040 1 05/11/15 00:00 MPR 13573 05/14/15 00:00 MIC 4481
Molybdenum ND mg/L 0.50 0.20 1 05/11/15 00:00 MPR 13573 05/14/15 00:00 MIC 4481
Nickel J0.042 mg/L 0.05 0.020 1 05/11/15 00:00 MPR 13573 05/14/15 00:00 MIC 4481
Selenium ND mg/L 0.50 0.20 105/11/1500:00 MPR 13573 05/14/15 00:00 MIC 4481
Silver ND mg/L 0.030 0.0060 1 05/11/15 00:00 MPR 13573 05/14/15 00:00 MIC 4481
Thallium ND mg/L 0.10 0.040 1 05/11/15 00:00 MPR 13573 05/14/15 00:00 MIC 4481
Vanadium 0.034 mg/L 0.02 0.0050 1 05/11115 00:00 MPR 13573 05/14/15 00:00 MIC 4481
Zinc 3.5 mg/L 0.20 0.10 1 05/11/15 00:00 MPR 13573 05/14/15 00:00 MIC 4481
Metals Analysis by ICP Prep Method: SW846 30508 Prep by: UK
Analytical Method: SW846 60108 Analyzed by: LM
Antimony ND mg/kg 2.0 1.5 1 05/06/15 00:00 MPR 13563 05/14/15 00:00 MIC4479
Arsenic ND mg/kg 2.0 1.0 1 05/06/15 00:00 MPR 13563 05/11/15 00:00 MIC4479
Barium 6.6 mg/kg 1.0 0.71 1 05/06/15 00:00 MPR 13563 05/11 /15 00:00 MIC4479
Beryllium ND mg/kg 0.20 0.15 1 05/06/15 00:00 MPR 13563 05/11/15 00:00 MIC4479
Cadmium J0.06 mg/kg 0.20 0.050 1 05/06/15 00:00 MPR 13563 05/11 /15 00:00 MIC 4479
Chromium J0.9 mg/kg 1.0 0.20 1 05/06/15 00:00 MPR 13563 05/11/15 00:00 MIC4479
Cobalt ND mg/kg 0.4 0.20 1 05/06/15 00:00 MPR 13563 05/11/15 00:00 MIC4479
Copper 14 mg/kg 2.0 0.20 1 05/06/15 00:00 MPR 13563 05/14/15 00:00 MIC 4479
6/18/2015 16:12 REPORT OF LABORATORY ANALYSIS Page 5 of 27
This report shall not be reproduced, except In full,
without the written consent of CALTEST ANALYTICAL LABORATORY
1885 North Kelly Road• Napa, California 9455 8
(707) 258-4000 • Fax (707) 226-1001 • e-mail: info@caltestlabs.com
DocuSign Envelope ID: 448F9D83-A76E-4EF1-9A95-3F616E43347D
NELAP/ORELAP Certification 4036
'
lr n.!test CA-ELAP Certification 1664
.. >...,,a.s.:. ~
\ N " , ,.,l "'\f 1 .,nnu '-·• 01n·
ll
ANALYTICAL RESULTS
Lab Order: 0050123
Project ID: NPDES QUARTERLY MAY 2015
Solid results are reported on a wet weight basis.
Lab ID Q050123004 Date Collected 5/4/2015 09:33 Matrix Solid
Sample ID E000766-01 BARSCREEN
RAGS
Date Received 5/5/2015 13:40 Results are expressed as wet weight values
Parameters Result Units R. L. MDL DF Prepared Batch Analyzed Batch Qua I
Lead ND mg/kg 1.0 0.50 1 05/06/15 00:00 MPR 13563 05/11/15 00:00 MIC4479
Molybdenum ND mg/kg 2.0 1.0 1 05/06/15 00:00 MPR 13563 05/11 /15 00:00 MIC4479
Nickel J0.93 mg/kg 1.0 0.30 1 05/06/15 00:00 MPR 13563 05/11/15 00:00 MIC4479
Selenium J1.5 mg/kg 2.0 0.81 1 05/06/15 00:00 MPR 13563 05/11 /15 00:00 MIC 4479
Silver J0.2 mg/kg 1.0 0.15 1 05/06/15 00:00 MPR 13563 05/11 /15 00:00 MIC 4479
Thallium ND mg/kg 2.0 0.71 1 05/06/15 00:00 MPR 13563 05/11 /15 00:00 MIC 4479
Vanadium 0.87 mg/kg 0.40 0.20 1 05/06/15 00:00 MPR 13563 05/11/15 00:00 MIC 4479
Zinc 60 mg/kg 4.0 1.0 1 05/06/15 00:00 MPR 13563 05/11/15 00:00 MIC4479
Asbestos Analysis -Solid Analytical Method: (per attached report) Asbestos Analysis -Solid
Analysis performed by EMSL Analytical, CA-ELAP Certification 1620. Refer to attached for original certificate of analysis.
Total Extractable Petroleum Prep Method: SW846 3541 Prep by: MDT
Hydrocarbon
Analytical Method: SW846 8015(MOD) Analyzed by: MDT
Diesel Fuel ND mg/kg 120 75 10 05/12/15 00:00 SPR6946 05/27/15 19:31 SFL 1703 5
TPH quantitated as Diesel 2830 mg/kg 120 75 10 05/12/15 00:00 SPR6946 05/27/15 19:31 SFL 1703
Fuel
o-Terphenyl (SS) 108 % 40-139 10 05/12/15 00:00 SPR 6946 05/27/15 19:31 SFL 1703
Semivolatile Organic Analysis Prep Method: SW846 3540 Prep by: MDT
Analytical Method: SW846 8270C Analyzed by: MDT
Acenaphthene ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR 6939 06/05/15 01:34 SMS 3755 3,4
Acenaphthylene ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR6939 06/05/15 01 :34 SMS 3755
Aniline ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR6939 06/05/15 01 :34 SMS 3755
Anthracene ND mg/kg 5.0 1.5 5 05/07/15 00:00 SPR6939 06/05/15 01 :34 SMS 3755
Benzidine ND mg/kg 10 7.5 5 05/07/15 00:00 SPR6939 06/05/15 01 :34 SMS 3755
Benzo(a)anthracene ND mg/kg 5.0 1.5 5 05/07/15 00:00 SPR6939 06/05/15 01 :34 SMS 3755
Benzo(a)pyrene ND mg/kg 5.0 1.5 5 05/07/15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
Benzo(b )fluoranthene ND mg/kg 5.0 1.5 5 05/07/15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
Benzo(g,h,i)perylene ND mg/kg 5.0 1.5 5 05/07/15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
Benzo(k)fluoranthene ND mg/kg 5.0 1.5 5 05/07/15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
Benzoic acid ND mg/kg 30 30 5 05/07/15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
Benzyl alcohol ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
Benzyl butyl phthalate ND mg/kg 5.0 1.5 5 05/07/15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
4-Bromophenyl phenyl ether ND mg/kg 5.0 3.0 5 05/07 /15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
Carbazole ND mg/kg 5.0 1.5 5 05/07/15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
4-Chloroaniline ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR6939 06/05/15 01 :34 SMS 3755
bis(2-Chloroethoxy) ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR6939 06/05/15 01 :34 SMS 3755
methane
bis(2-Chloroethyl) ether ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR6939 06/05/15 01 :34 SMS 3755
bis(2-Chloroisopropyl) ether ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR6939 06/05/15 01 :34 SMS 3755
4-Chloro-3-methylphenol ND mg/kg 5.0 4.5 5 05/07/15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
2-Chloronaphthalene ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
2-Chlorophenol ND mg/kg 5.0 4.5 5 05/07/15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
4-Chlorophenyl phenyl ether ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
6/18/2015 16:12 REPORT OF LABORATORY ANALYSIS Page 6 of 27
This report shall not be reproduced, except in full,
without the written consent of CALTEST ANALYTICAL LABORATORY
,@·1-~,~ 1885 North Kelly Road• Napa, California 94558 ~z") :1r~. •• ~nelac\, (707) 258-4000 • Fax (707) 226-1001 • e-mail: info@caltestlabs.com ,.,
DocuSign Envelope ID: 448F9D83-A76E-4EF1-9A95-3F616E43347D
NELAP/ORELAP Certification 4036 'l_ Caltest CA-ELAP Certification 1664
',\N/\1\'lll"·\I I IIIOIIAIOH\' EVISEDII ENVIRONMENTAL ANALYSES
ANALYTICAL RESULTS
Lab Order: 0050123
Project ID: NPDES QUARTERLY MAY 2015
Solid results are reported on a wet weight basis.
Lab ID Q050123004 Date Collected 5/4/2015 09:33 Matrix Solid
Sample ID E000766-01 BARSCREEN
RAGS
Date Received 5/5/2015 13:40 Results are expressed as wet weight values
Parameters Result Units R. L. MDL DF Prepared Batch Analyzed Batch Qua I
Chrysene ND mg/kg 5.0 1.5 5 05/07/15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
Total Cresci J9.7 mg/kg 10 9.0 5 05/07/15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
Dibenzo(a,h)anthracene ND mg/kg 5.0 1.5 5 05/07/15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
Dibenzofuran ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
1,2-Dichlorobenzene ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
1,3-Dichlorobenzene ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
1,4-Dichlorobenzene ND mg/kg 5.0 3.0 5 05/07 /15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
3,3'-Dichlorobenzidine ND mg/kg 5.0 4.5 5 05/07/15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
2,4-Dichlorophenol ND mg/kg 5.0 4.5 5 05/07/15 00:00 SPR6939 06/05/15 01 :34 SMS 3755
Diethylphthalate ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR6939 06/05/15 01 :34 SMS 3755
2,4-Dimethylphenol ND mg/kg 5.0 4.5 5 05/07/15 00:00 SPR6939 06/05/15 01 :34 SMS 3755
Dimethylphthalate ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR6939 06/05/15 01 :34 SMS 3755
Di-n-butylphthalate ND mg/kg 5.0 1.5 5 05/07/15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
2,4-Dinitrophenol ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
2,4-Dinitrotoluene ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
2,6-Dinitrotoluene ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
Di-n-octylphthalate ND mg/kg 5.0 1.5 5 05/07 /15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
1,2-Diphenylhydrazine I ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR6939 06/05/15 01 :34 SMS 3755
Azobenzene
bis(2-Ethylhexyl) phthalate ND mg/kg 5.0 4.5 5 05/07/15 00:00 SPR6939 06/05/15 01 :34 SMS 3755
Fluoranthene ND mg/kg 5.0 1.5 5 05/07/15 00:00 SPR6939 06/05/15 01 :34 SMS 3755
Fluorene ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
Hexachlorobenzene ND mg/kg 5.0 1.5 5 05/07/15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
Hexachlorobutadiene ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
Hexachlorocyclo pentadiene ND mg/kg 5.0 1.5 5 05/07/15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
Hexachloroethane ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR6939 06/05/15 01 :34 SMS 3755
lndeno(1,2,3-cd)pyrene ND mg/kg 5.0 1.5 5 05/07/15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
lsophorone ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR6939 06/05/15 01 :34 SMS 3755
2-Methyl-4,6-dinitrophenol ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR6939 06/05/15 01 :34 SMS 3755
2-Methylnaphthalene ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
2-Methylphenol (o-Cresol) ND mg/kg 5.0 4.5 5 05/07/15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
3 & 4-Methylphenol(m&p 9.7 mg/kg 5.0 4.5 5 05/07/15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
Cresci)
Naphthalene ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
2-Nitroaniline ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
3-Nitroaniline ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR6939 06/05/15 01 :34 SMS 3755
4-Nitroaniline ND mg/kg 5.0 1.5 5 05/07 /15 00:00 SPR6939 06/05/15 01 :34 SMS 3755
Nitrobenzene ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR6939 06/05/15 01 :34 SMS 3755
2-Nitrophenol ND mg/kg 5.0 4.5 5 05/07/15 00:00 SPR6939 06/05/15 01 :34 SMS 3755
4-Nitrophenol ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
N-Nitrosodimethylamine ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
N-Nitroso-di-n-propylamine ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
N-Nitrosodiphenylamine ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
Pentachlorophenol ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
Phenanthrene ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
6/18/2015 16:12 REPORT OF LABORATORY ANALYSIS Page 7 of 27
This report shall not be reproduced, except In full,
without the written consent of CALTEST ANALYTICAL LABORATORY
",~oc~ 1885 North Kelly Road• Napa, California 94558 lt1elc~~ n
(707) 258-4000 • Fax (707) 226-1001 • e-mail: info@caltestlabs.com '-.,
DocuSign Envelope ID: 448F9D83-A76E-4EF1-9A95-3F61 6E43347D
NELAP/ORELAP Certification 4036 ~-.:r.
\-i··-~-Caltest CA-ELAP Certification 1664
·~~-1. --~ ~ti .\r,,,:.\I \"lf(",\I l \111>1: \IUH\
N lll0NMHN1'AI; ANAI.Y ·es
ANALYTICAL RESULTS
Lab Order: 0050123
Project ID: NPDES QUARTERLY MAY 2015
Solid results are reported on a wet weight basis.
Lab ID Q050123004 Date Collected 5/4/2015 09:33 Matrix Solid
Sample ID E000766-01 BARSCREEN
RAGS
Date Received 5/5/2015 13:40 Results are expressed as wet weight values
Parameters Result Units R. L. MDL DF Prepared Batch Analyzed Batch Qua I
Phenol ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
Pyrene ND mg/kg 5.0 1.5 5 05/07/15 00:00 SPR6939 06/05/15 01 :34 SMS 3755
Pyridine ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR6939 06/05/15 01 :34 SMS 3755
1,2,4-Trichlorobenzene ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
2,4,5-Trichlorophenol ND mg/kg 5.0 4.5 5 05/07/15 00:00 SPR6939 06/05/15 01 :34 SMS 3755
2,4,6-Trichlorophenol ND mg/kg 5.0 4.5 5 05/07/15 00:00 SPR6939 06/05/15 01 :34 SMS 3755
2-Fluorobiphenyl (SS) 81 % 10-149 5 05/07/15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
2-Fluorophenol (SS) 50% 47-105 5 05/07/15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
Nitrobenzene-d5 (SS) 70% 57-108 5 05/07/15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
Phenol-d6 (SS) 75% 58-97 5 05/07/15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
Terphenyl-d14 (SS) 82% 32-120 5 05/07/15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
2,4,6-Tribromophenol (SS) 130 % 26-143 5 05/07/15 00:00 SPR 6939 06/05/15 01 :34 SMS 3755
Volatile Organic Analysis Analytical Method: SW846 50308/82608 Analyzed by: AN
Benzene ND mg/kg 0.025 0.010 05/07/15 18:57 VMS 3245 4
Bromobenzene ND mg/kg 0.025 0.010 05/07/15 18:57 VMS 3245
Bromochloromethane ND mg/kg 0.025 0.015 05/07/15 18:57 VMS 3245
Bromodichloromethane ND mg/kg 0.025 0.010 05/07/15 18:57 VMS3245
Bromoform ND mg/kg 0.025 0.0050 05/07/15 18:57 VMS 3245
Bromomethane (Methyl ND mg/kg 0.10 0.020 05/07/15 18:57 VMS 3245
Bromide)
n-Butylbenzene ND mg/kg 0.025 0.010 05/07/15 18:57 VMS 3245
sec-Butylbenzene ND mg/kg 0.025 0.010 05/07/15 18:57 VMS 3245
tert-Butylbenzene ND mg/kg 0.025 0.010 05/07/1518:57 VMS 3245
Carbon tetrachloride ND mg/kg 0.025 0.010 05/07/15 18:57 VMS 3245
Chlorobenzene ND mg/kg 0.025 0.010 05/07/15 18:57 VMS 3245
Chloroethane (Ethyl ND mg/kg 0.10 0.015 05/07 /15 18:57 VMS 3245
Chloride)
Chloroform ND mg/kg 0.025 0.010 05/07/15 18:57 VMS 3245
Chloromethane(Methyl ND mg/kg 0.10 0.010 05/07/1518:57 VMS 3245
Chloride)
2-Chlorotoluene ND mg/kg 0.025 0.010 05/07/15 18:57 VMS 3245
4-Chlorotoluene ND mg/kg 0.025 0.010 05/07 /15 18:57 VMS 3245
Dibromochloromethane ND mg/kg 0.025 0.0050 05/07/15 18:57 VMS 3245
1,2-Dibromo-3-ND mg/kg 0.025 0.010 05/07/15 18:57 VMS 3245
chloropropane
1,2-Dibromoethane (EDB) ND mg/kg 0.025 0.0050 05/07/15 18:57 VMS 3245
Dibromomethane ND mg/kg 0.025 0.010 05/07/15 18:57 VMS 3245
1,2-Dichlorobenzene ND mg/kg 0.025 0.010 05/07 /15 18:57 VMS 3245
1,3-Dichlorobenzene ND mg/kg 0.025 0.010 05/07 /15 18:57 VMS 3245
1,4-Dichlorobenzene ND mg/kg 0.025 0.0050 05/07/15 18:57 VMS 3245
Dichlorodifluoromethane (F-ND mg/kg 0.050 0.010 05/07/15 18:57 VMS 3245
12)
1, 1-Dlchloroethane ND mg/kg 0.025 0.010 05/07/1518:57 VMS 3245
1,2-Dichloroethane (EDC) ND mg/kg 0.025 0.0050 05/07/15 18:57 VMS 3245
1, 1-Dichloroethene ND mg/kg 0.025 0.010 05/07 /15 18:57 VMS 3245
cis-1,2-Dichloroethene ND mg/kg 0.025 0.010 05/07/15 18:57 VMS 3245
6/18/2015 16:12 REPORT OF LABORATORY ANALYSIS Page 8 of 27
This report shall not be reproduced, except in full,
without the written consent of CALTEST ANALYTICAL LABORATORY
~h 1885 North Kelly Road• Napa, California 94558 .#' :l's n
I I' . ,., fneac~ (707) 258-4000 • Fax (707) 226-1001 • e-mail: info@caltestlabs.com
DocuSign Envelope ID: 448F9D83-A76E-4EF1-9A95-3F616E43347D
NELAP/ORELAP Certification 4036
~rt .. Caltest '\,·11'" ">t;'l \N,\I \"11(',\I I \1101< \l(ltO
CA-ELAP Certification 1664
VISED!I
ANALYTICAL RESULTS
Lab Order: 0050123
Project ID: NPDES QUARTERLY MAY 2015
Solid results are reported on a wet weight basis.
Lab ID Q050123004 Date Collected 5/4/2015 09:33 Matrix Solid
Sample ID E000766-01 BARSCREEN
RAGS
Date Received 5/5/2015 13:40 Results are expressed as wet weight values
Parameters Result Units R. L. MDL OF Prepared Batch Analyzed Batch Qua I
trans-1,2-Dichloroethene ND mg/kg 0.025 0.010 05/07/15 18:57 VMS 3245
1,2-Dichloropropane ND mg/kg 0.025 0.010 05/07/15 18:57 VMS 3245
1,3-Dlchloropropane ND mg/kg 0.025 0.010 05/07/15 18:57 VMS 3245
2,2-Dichloropropane ND mg/kg 0.025 0.010 05/07 /15 18:57 VMS 3245
1, 1-Dichloropropene ND mg/kg 0.025 0.010 05/07 /15 18:57 VMS 3245
Dichlorotrifluoroethane ND mg/kg 0.025 0.0050 05/07 /15 18:57 VMS 3245
(F123)
Ethyl benzene ND mg/kg 0.025 0.010 05/07 /15 18:57 VMS 3245
Hexachlorobutadiene NO mg/kg 0.025 0.010 05/07/15 18:57 VMS 3245
4-lsopropyltoluene ND mg/kg 0.025 0.010 05/07/1518:57 VMS 3245
Methyl tert-butyl ether ND mg/kg 0.025 0.010 05/07/15 18:57 VMS 3245
(MTBE)
Methylene chloride ND mg/kg 0.15 0.0050 05/07/1518:57 VMS 3245
Naphthalene ND mg/kg 0.025 0.010 05/07/15 18:57 VMS 3245
n-Propylbenzene ND mg/kg 0.025 0.010 05/07 /15 18:57 VMS 3245
Styrene ND mg/kg 0.025 0.010 05/07/15 18:57 VMS 3245
1, 1, 1,2-Tetrachloroethane ND mg/kg 0.025 0.010 05/07/15 18:57 VMS 3245
1, 1,2,2-Tetrachloroethane NO mg/kg 0.025 0.010 05/07/15 18:57 VMS 3245
Tetrachloroethene (PCE) NO mg/kg 0.025 0.010 05/07/1518:57 VMS 3245
Toluene ND mg/kg 0.025 0.0050 05/07/15 18:57 VMS 3245
1,2,3-Trichlorobenzene ND mg/kg 0.025 0.010 05/07/15 18:57 VMS 3245
1,2.4-Trichlorobenzene ND mg/kg 0.025 0.010 05/07/15 18:57 VMS 3245
1, 1,2-Trichloroethane NO mg/kg 0.025 0.0050 05/07/15 18:57 VMS 3245
1, 1, 1-Trichloroethane (TCA) ND mg/kg 0.025 0.010 05/07/15 18:57 VMS 3245
Trichloroethane (TCE) NO mg/kg 0.025 0.010 05/07 /15 18:57 VMS 3245
Trichlorofluoromethane (F-ND mg/kg 0.025 0.020 05/07/15 18:57 VMS 3245
11)
1,2,3-Trlchloropropane ND mg/kg 0.025 0.010 05/07/15 18:57 VMS 3245
Trichlorotrifluorethane ND mg/kg 0.050 0.010 05/07/1518:57 VMS 3245
(F113)
1,2.4-Trimethylbenzene ND mg/kg 0.025 0.010 05/07/15 18:57 VMS 3245
1,3,5-Trlmethylbenzene ND mg/kg 0.025 0.010 05/07/15 18:57 VMS 3245
Vinyl chloride ND mg/kg 0.025 0.015 05/07 /15 18:57 VMS 3245
Xylenes, total NO mg/kg 0.025 0.0050 05/07/15 18:57 VMS 3245
4-Bromofluorobenzene (SS) 92% 74-130 05/07/15 18:57 VMS 3245
Dibromofluoromethane (SS) 111 % 69-129 05/07/15 18:57 VMS 3245
1,2-Dichloroethane-d4 (SS) 116 % 61-133 05/07/15 18:57 VMS 3245
Toluene-dB (SS) 103% 71-135 05/07/1518:57 VMS 3245
Cyanide, Total Analysis Analytical Method: SW846 9012A Analyzed by: BCP
Cyanide 0.094 mg/kg 0.080 0.080 05/09/15 17:05 wco 10778
6/18/2015 16:12 REPORT OF LABORATORY ANALYSIS Page 9 of 27
This report shall not be reproduced, except in full,
without the written consent of CAL TEST ANALYTICAL LABORATORY
1885 North Kelly Road• Napa, California 94558
(707) 258-4000 • Fax (707) 226-1001 • e-mail: info@caltestlabs.com
DocuSign Envelope ID: 448F9083-A76E-4EF1-9A95-3F616E43347D
NELAP/ORELAP Certification 4036 ~t .. Caltest ,r. .
CA-ELAP Certification 1664
·~: ,'•"I··~ ... "'~"itli \S.\l YflC.\I I \HOH \'I I Ht\"
E N Ill N ;t ··NT.-\l. NA LY!rnS II REVISED II
ANALYTICAL RESULTS
Lab Order: 0050123
Project ID: NPDES QUARTERLY MAY 2015
Solid results are reported on a wet weight basis.
Lab ID Q050123005 Date Collected 5/4/2015 09:35 Matrix Solid
Sample ID E000767·01 GRIT Date Received 5/5/2015 13:40 Results are expressed as wet weight values
Parameters Result Units R. L. MDL OF Prepared Batch Analyzed Batch Qua I
Mercury Analysis, STLC, Low Level Prep Method: SW846 7470ALow Level Prep by: UK
Analytical Method: SW846 7 4 70A Low Level Analyzed by: LM
Mercury ND ug/L 0.50 0.30 1 05/12/15 00:00 MPR 13577 05/13/15 13:56 MHG 4968
Mercury Analysis Prep Method: SW846 7471A Prep by: UK
Analytical Method: SW846 7471A Analyzed by: LM
Mercury 0.099 mg/kg 0.020 0.00079 1 05/06/15 00:00 MPR 13565 05/07/15 13:52 MHG4963
Metals Analysis by ICP, STLC Prep Method: SW846 3010 Prep by: UK
Analytical Method: SW846 60108 (Leachate) Analyzed by: LM
Antimony ND mg/L 0.10 0.040 1 05/11 /15 00:00 MPR 13573 05/14/15 00:00 MIC 4481
Arsenic J0.055 mg/L 0.10 0.050 105/11/1500:00 MPR 13573 05/14/15 00:00 MIC 4481
Barium 1.4 mg/L 0.15 0.070 1 05/11/15 00:00 MPR 13573 05/14/15 00:00 MIC 4481
Beryllium ND mg/L 0.010 0.0050 1 05/11/15 00:00 MPR 13573 05/14/15 00:00 MIC4481
Cadmium J0.0043 mg/L 0.010 0.0040 105/11/1500:00 MPR 13573 05/14/15 00:00 MIC 4481
Chromium 0.11 mg/L 0.10 0.050 105/11/1500:00 MPR 13573 05/14/15 00:00 MIC 4481
Cobalt ND mg/L 0.050 0.020 1 05/11 /15 00:00 MPR 13573 05/14/15 00:00 MIC 4481
Copper ND mg/L 0.10 0.030 1 05/11 /15 00:00 MPR 13573 05/14/15 00:00 MIC 4481
Lead ND mg/L 0.10 0.040 105/11/1500:00 MPR 13573 05/14/15 00:00 MIC 4481
Molybdenum ND mg/L 0.50 0.20 105/11/1500:00 MPR 13573 05/14/15 00:00 MIC4481
Nickel 0.13 mg/L 0.05 0.020 1 05/11 /15 00:00 MPR 13573 05/14/15 00:00 MIC 4481
Selenium ND mg/L 0.50 0.20 1 05/11 /15 00:00 MPR 13573 05/14/15 00:00 MIC 4481
Sliver ND mg/L 0.030 0.0060 1 05/11/15 00:00 MPR 13573 05/14/15 00:00 MIC 4481
Thallium ND mg/L 0.10 0.040 1 05/11/15 00:00 MPR 13573 05/14/15 00:00 MIC 4481
Vanadium 0.066 mg/L 0.02 0.0050 105/11/1500:00 MPR 13573 05/14/15 00:00 MIC 4481
Zinc 2.9 mg/L 0.20 0.10 1 05/11/15 00:00 MPR 13573 05/14/15 00:00 MIC 4481
Metals Analysis by ICP Prep Method: SW846 30508 Prep by: UK
Analytical Method: SW846 60108 Analyzed by: LM
Antimony ND mg/kg 2.0 1.5 1 05/06/15 00:00 MPR 13563 05/14/15 00:00 MIC4479
Arsenic ND mg/kg 2.0 1.0 1 05/06/15 00:00 MPR 13563 05/11/15 00:00 MIC4479
Barium 20 mg/kg 1.0 0.70 1 05/06/15 00:00 MPR 13563 05/11/15 00:00 MIC4479
Beryllium ND mg/kg 0.20 0.15 1 05/06/15 00:00 MPR 13563 05/11/15 00:00 MIC 4479
Cadmium J0.09 mg/kg 0.20 0.050 1 05/06/15 00:00 MPR 13563 05/11 /15 00:00 MIC4479
Chromium 3.0 mg/kg 1.0 0.20 1 05/06/15 00:00 MPR 13563 05/11/15 00:00 MIC4479
Cobalt 0.6 mg/kg 0.4 0.20 1 05/06/15 00:00 MPR 13563 05/11/15 00:00 MIC4479
Copper 40 mg/kg 2.0 0.20 1 05/06/15 00:00 MPR 13563 05/14/15 00:00 MIC 4479
Lead 6.4 mg/kg 1.0 0.50 1 05/06/15 00:00 MPR 13563 05/11 /15 00:00 MIC4479
Molybdenum ND mg/kg 2.0 1.0 1 05/06/15 00:00 MPR 13563 05/11/15 00:00 MIC4479
Nickel 3.4 mg/kg 1.0 0.30 1 05/06/15 00:00 MPR 13563 05/11/15 00:00 MIC4479
Selenium ND mg/kg 2.0 0.80 1 05/06/15 00:00 MPR 13563 05/11/15 00:00 MIC4479
Silver J0.5 mg/kg 1.0 0.15 1 05/06/15 00:00 MPR 13563 05/11/15 00:00 MIC4479
Thallium ND mg/kg 2.0 0.70 1 05/06/15 00:00 MPR 13563 05/11/15 00:00 MIC4479
Vanadium 2.6 mg/kg 0.40 0.20 1 05/06/15 00:00 MPR 13563 05/11/15 00:00 MIC4479
Zinc 96 mg/kg 4.0 1.0 1 05/06/15 00:00 MPR 13563 05/11/15 00:00 MIC 4479
Asbestos Analysis • Solid Analytical Method: (per attached report) Asbestos Analysis • Solid
6/18/2015 16:12 REPORT OF LABORATORY ANALYSIS Page 10 of 27
This report shall not be reproduced, except In full,
without the written consent of CAL TEST ANALYTICAL LABORATORY
~"!~ 1885 North Kelly Road• Napa, California 94558 ~)VI kh.'-i) i nelac~ (707) 258-4000 • Fax (707) 226-1001 • e-mail: info@caltestlabs.com
DocuSign Envelope ID: 448F9D83-A76E-4EF1-9A95-3F616E43347D
NELAP/ORELAP Certification 4036 tr~ Caltest
-:J11=.-···"!~ .r\1';,\l.\l"f(,\I I \UOll\'IOU\
CA-ELAP Ce1iification 1664
011
ANALYTICAL RESULTS
Lab Order: 0050123
Project ID: NPDES QUARTERLY MAY 2015
Solid results are reported on a wet weight basis.
Lab ID Q050123005 Date Collected 5/4/2015 09:35 Matrix Solid
Sample ID E000767-01 GRIT Date Received 5/5/2015 13:40 Results are expressed as wet weight values
Parameters Result Units R.L. MDL OF Prepared Batch Analyzed Batch Qua I
Analysis performed by EMSL Analytical, CA-ELAP Certification 1620. Refer to attached for original certificate of analysis.
Total Extractable Petroleum Prep Method: SW846 3541 Prep by: MDT
Hydrocarbon
Analytical Method: SW846 8015(MOD) Analyzed by: MDT
Diesel Fuel ND mg/kg 60 38 5 05/12/15 00:00 SPR 6946 05/27 /15 20: 17 SFL 1703 5
TPH quantitated as Diesel 1720 mg/kg 60 38 5 05/12/15 00:00 SPR6946 05/27/15 20:17 SFL 1703
Fuel
o-Terphenyl (SS) 102 % 40-139 5 05/12/15 00:00 SPR6946 05/27/15 20:17 SFL 1703
Semlvolatile Organic Analysis Prep Method: SW846 3540 Prep by: MDT
Analytical Method: SW846 8270C Analyzed by: MDT
Acenaphthene ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR 6939 06/05/15 02:12 SMS 3755 4,3
Acenaphthylene ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR 6939 06/05/15 02: 12 SMS 3755
Aniline ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR 6939 06/05/15 02:12 SMS 3755
Anthracene ND mg/kg 5.0 1.5 5 05/07/15 00:00 SPR6939 06/05/15 02:12 SMS 3755
Benzidine ND mg/kg 10 7.5 5 05/07/15 00:00 SPR6939 06/05/15 02: 12 SMS 3755
Benzo(a)anthracene ND mg/kg 5.0 1.5 5 05/07/15 00:00 SPR 6939 06/05/15 02:12 SMS 3755
Benzo(a)pyrene ND mg/kg 5.0 1.5 5 05/07/15 00:00 SPR 6939 06/05/15 02:12 SMS 3755
Benzo(b )fluoranthene ND mg/kg 5.0 1.5 5 05/07/15 00:00 SPR6939 06/05/15 02:12 SMS 3755
Benzo(g,h,i)perylene ND mg/kg 5.0 1.5 5 05/07/15 00:00 SPR 6939 06/05/15 02:12 SMS 3755
Benzo(k)fluoranthene ND mg/kg 5.0 1.5 5 05/07/15 00:00 SPR 6939 06/05/15 02:12 SMS 3755
Benzoic acid ND mg/kg 30 30 5 05/07/15 00:00 SPR6939 06/05/15 02:12 SMS 3755
Benzyl alcohol ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR6939 06/05/15 02: 12 SMS 3755
Benzyl butyl phthalate ND mg/kg 5.0 1.5 5 05/07/15 00:00 SPR 6939 06/05/15 02:12 SMS 3755
4-Bromophenyl phenyl ether ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR6939 06/05/15 02:12 SMS 3755
Carbazole ND mg/kg 5.0 1.5 5 05/07/15 00:00 SPR6939 06/05/15 02:12 SMS 3755
4-Chloroaniline ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR 6939 06/05/15 02: 12 SMS 3755
bis(2-Chloroethoxy) ND mg/kg 5.0 3.0 5 05/07 /15 00:00 SPR 6939 06/05/15 02:12 SMS 3755
methane
bis(2-Chloroethyl) ether ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR6939 06/05/15 02:12 SMS 3755
bis(2-Chloroisopropyl) ether ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR 6939 06/05/15 02: 12 SMS 3755
4-Chloro-3-methylphenol ND mg/kg 5.0 4.5 5 05/07/15 00:00 SPR 6939 06/05/15 02: 12 SMS 3755
2-Chloronaphthalene ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR6939 06/05/15 02:12 SMS 3755
2-Chlorophenol ND mg/kg 5.0 4.5 5 05/07/15 00:00 SPR 6939 06/05/15 02:12 SMS 3755
4-Chlorophenyl phenyl ether ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR 6939 06/05/15 02: 12 SMS 3755
Chrysene ND mg/kg 5.0 1.5 5 05/07/15 00:00 SPR6939 06/05/15 02: 12 SMS 3755
Total Cresol ND mg/kg 10 9.0 5 05/07/15 00:00 SPR6939 06/05/15 02: 12 SMS 3755
Dibenzo(a,h)anthracene ND mg/kg 5.0 1.5 5 05/07 /15 00:00 SPR 6939 06/05/15 02:12 SMS 3755
Dibenzofuran ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR 6939 06/05/15 02:12 SMS 3755
1,2-Dichlorobenzene ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR6939 06/05/15 02:12 SMS 3755
1,3-Dichlorobenzene ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR 6939 06/05/15 02:12 SMS 3755
1,4-Dichlorobenzene ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR 6939 06/05/15 02:12 SMS 3755
3,3'-Dichlorobenzidine ND mg/kg 5.0 4.5 5 05/07/15 00:00 SPR6939 06/05/15 02: 12 SMS 3755
2,4-Dichlorophenol ND mg/kg 5.0 4.5 5 05/07/15 00:00 SPR 6939 06/05/15 02:12 SMS 3755
Diethylphthalate ND mg/kg 5.0 3.0 5 05/07 /15 00:00 SPR 6939 06/05/15 02:12 SMS 3755
6/18/2015 16:12 REPORT OF LABORATORY ANALYSIS Page 11 of 27
This report shall not be reproduced, except in full,
without the written consent of CALTEST ANALYTICAL LABORATORY
~~· • .'~<)~ 1885 North Kelly Road• Napa, California 94558 ey_~.-:· y,~ ...
"'' I I ~ ' \ii Hine act (707) 258-4000 • Fax (707) 226-1001 • e-mail: info@caltestlabs.com
DocuSign Envelope ID: 448F9D83-A76E-4EF1-9A95-3F616E43347D
NELAP/ORELAP Certification 4036 ~~ Caltest ' \' ~~:~) ,\N.\I \"l "'"' L\111111,\ rrnl\'
CA-ELAP Certification 1664
-irl'Jvrncri'J MT.'f,I' ;\L ANA ~ -
ANALYTICAL RESULTS
Lab Order: 0050123
Project JD: NPDES QUARTERLY MAY 2015
Solid results are reported on a wet weight basis.
Lab ID Q050123005 Date Collected 5/4/2015 09:35 Matrix Solid
Sample ID E000767-01 GRIT Date Received 5/5/2015 13:40 Results are expressed as wet weight values
Parameters Result Units R. L. MDL OF Prepared Batch Analyzed Batch Qua I
2.4-Dimethylphenol ND mg/kg 5.0 4.5 5 05/07/15 00:00 SPR 6939 06/05/15 02:12 SMS 3755
Dimethylphthalate ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR6939 06/05/15 02:12 SMS 3755
Di-n-butylphthalate ND mg/kg 5.0 1.5 5 05/07/15 00:00 SPR6939 06/05/15 02: 12 SMS 3755
2,4-Dinitrophenol ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR6939 06/05/15 02: 12 SMS 3755
2.4-Dinitrotoluene ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR 6939 06/05/15 02:12 SMS 3755
2,6-Dinitrotoluene ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR6939 06/05/15 02:12 SMS 3755
Di-n-octylphthalate ND mg/kg 5.0 1.5 5 05/07/15 00:00 SPR6939 06/05/15 02:12 SMS 3755
1,2-Diphenylhydrazine I ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR 6939 06/05/15 02:12 SMS 3755
Azobenzene
bis(2-Ethylhexyl) phthalate ND mg/kg 5.0 4.5 5 05/07/15 00:00 SPR 6939 06/05/15 02:12 SMS 3755
Fluoranthene ND mg/kg 5.0 1.5 5 05/07/15 00:00 SPR6939 06/05/15 02:12 SMS 3755
Fluorene ND mg/kg 5.0 3.0 5 05107 /15 00:00 SPR6939 06105/15 02:12 SMS 3755
Hexachlorobenzene ND mg/kg 5.0 1.5 5 05107/15 00:00 SPR6939 06/05115 02:12 SMS 3755
Hexachlorobutadiene ND mg/kg 5.0 3.0 5 05107/15 00:00 SPR 6939 06/05/15 02:12 SMS 3755
Hexachlorocyclo pentadiene ND mg/kg 5.0 1.5 5 05/07/15 00:00 SPR 6939 06/05/15 02:12 SMS 3755
Hexachloroethane ND mg/kg 5.0 3.0 5 05107115 00:00 SPR6939 06105115 02:12 SMS 3755
lndeno(1,2,3-cd)pyrene ND mg/kg 5.0 1.5 5 05/07115 00:00 SPR6939 06105/15 02: 12 SMS 3755
lsophorone ND mg/kg 5.0 3.0 5 05107/15 00:00 SPR 6939 06/05115 02:12 SMS 3755
2-Methyl-4,6-dinitrophenol ND mg/kg 5.0 3.0 5 05107/15 00:00 SPR 6939 06105/15 02: 12 SMS 3755
2-Methylnaphthalene ND mg/kg 5.0 3.0 5 05/07115 00:00 SPR6939 06/05115 02:12 SMS 3755
2-Methylphenol (o-Cresol) ND mg/kg 5.0 4.5 5 05/07115 00:00 SPR6939 06/05115 02:12 SMS 3755
3 & 4-Methylphenol(m&p 7.7 mg/kg 5.0 4.5 5 05/07/15 00:00 SPR 6939 06/05/15 02:12 SMS 3755
Cresol)
Naphthalene ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR6939 06/05/15 02:12 SMS 3755
2-Nitroaniline ND mg/kg 5.0 3.0 5 05/07115 00:00 SPR6939 06105/15 02: 12 SMS 3755
3-Nitroaniline ND mg/kg 5.0 3.0 5 05107/15 00:00 SPR 6939 06105/15 02: 12 SMS 3755
4-Nitroaniline ND mg/kg 5.0 1.5 5 05/07115 00:00 SPR 6939 06/05115 02:12 SMS 3755
Nitrobenzene ND mg/kg 5.0 3.0 5 05/07115 00:00 SPR6939 06/05115 02:12 SMS 3755
2-Nitrophenol ND mg/kg 5.0 4.5 5 05107/15 00:00 SPR6939 06/05/15 02: 12 SMS 3755
4-Nitrophenol ND mg/kg 5.0 3.0 5 05107/15 00:00 SPR 6939 06105/15 02:12 SMS 3755
N-Nitrosodimethylamine ND mg/kg 5.0 3.0 5 05/07115 00:00 SPR 6939 06/05115 02:12 SMS 3755
N-Nitroso-di-n-propylamine ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR6939 06/05/15 02:12 SMS 3755
N-Nitrosodiphenylamine ND mg/kg 5.0 3.0 5 05/07115 00:00 SPR6939 06/05115 02: 12 SMS 3755
Pentachlorophenol ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR6939 06/05115 02:12 SMS 3755
Phenanthrene ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR 6939 06105/15 02: 12 SMS 3755
Phenol ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR 6939 06105/15 02:12 SMS 3755
Pyrene J2.0 mg/kg 5.0 1.5 5 05107115 00:00 SPR6939 06105115 02:12 SMS 3755
Pyridine ND mg/kg 5.0 3.0 5 05/07115 00:00 SPR6939 06105/15 02:12 SMS 3755
1,2,4-Trichlorobenzene ND mg/kg 5.0 3.0 5 05/07/15 00:00 SPR 6939 06105/15 02: 12 SMS 3755
2.4,5-Trichlorophenol ND mg/kg 5.0 4.5 5 05/07/15 00:00 SPR 6939 06105/15 02:12 SMS 3755
2,4,6-Trichlorophenol ND mg/kg 5.0 4.5 5 05/07115 00:00 SPR6939 06/05115 02:12 SMS 3755
2-Fluorobiphenyl (SS) 75% 10-149 5 05/07115 00:00 SPR6939 06105115 02:12 SMS 3755
2-Fluorophenol (SS) 54% 47-105 5 05107/15 00:00 SPR 6939 06105/15 02: 12 SMS 3755
Nitrobenzene-d5 (SS) 61 % 57-108 5 05107115 00:00 SPR 6939 06/05/15 02:12 SMS 3755
Phenol-dB (SS) 65% 58-97 5 05/07115 00:00 SPR6939 06/05/15 02:12 SMS 3755
Terphenyl-d14 (SS) 94% 32-120 5 05/07/15 00:00 SPR 6939 06/05115 02:12 SMS 3755
6/18/2015 16:12 REPORT OF LABORATORY ANALYSIS Page 12 of 27
This report shall not be reproduced, except in full,
without the written consent of CAL TEST ANALYTICAL LABORATORY
""~ li!, ,, ... ~ 1885 North Kelly Road• Napa, California 94558 •'" shellc:·t (707) 258-4000 • Fax (707) 226-1001 • e-mail: info@caltestlabs.com ~,
DocuSign Envelope ID: 448F9D83-A76E-4EF1-9A95-3F616E433470
NELAP/ORELAP Certification 4036 t.l'J ":~~~-Caltest ~ A"-AI, rlCAI I ,\ll<llUIOll'
CA-ELAP Certification 1664
II REVISED I!
ANALYTICAL RESULTS
Lab Order: 0050123
Project ID: NPDES QUARTERLY MAY 2015
Solid results are reported on a wet weight basis.
Lab ID Q050123005 Date Collected 5/4/2015 09:35 Matrix Solid
Sample ID E000767-01 GRIT Date Received 5/5/2015 13:40 Results are expressed as wet weight values
Parameters Result Units R. L. MDL DF Prepared Batch Analyzed Batch Qua I
2,4,6-Tribromophenol (SS)
Volatile Organic Analysis
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane (Methyl
Bromide)
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane (Ethyl
Chloride)
Chloroform
Chloromethane(Methyl
Chloride)
2-Chlorotoluene
4-Chlorotoluene
Dibromochloromethane
1,2-Dibromo-3-
chloropropane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane (F-
12)
1, 1-Dichloroethane
1,2-Dichloroethane (EDC)
1, 1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1, 1-Dichloropropene
Dichlorotrifluoroethane
(F123)
Ethylbenzene
Hexachlorobutadiene
4-lsopropyltoluene
Methyl tert-butyl ether
(MTBE)
6/18/2015 16:12
122 % 26-143 5 05/07/15 00:00 SPR6939
Analytical Method: SW846 50308/82608
ND mg/kg 0.025 0.010
ND mg/kg 0.025 0.010
ND mg/kg 0.025 0.015
ND mg/kg 0.025 0.010
ND mg/kg 0.025 0.0050
ND mg/kg 0.10 0.020
ND mg/kg 0.025 0.010
ND mg/kg 0.025 0.010
ND mg/kg 0.025 0.010
ND mg/kg 0.025 0.010
ND mg/kg 0.025 0.010
ND mg/kg 0.10 0.015
ND mg/kg 0.025 0.010
ND mg/kg 0.10 0.010
ND mg/kg 0.025 0.010
ND mg/kg 0.025 0.010
ND mg/kg 0.025 0.0050
ND mg/kg 0.025 0.010
ND mg/kg 0.025 0.0050
ND mg/kg 0.025 0.010
ND mg/kg 0.025 0.010
ND mg/kg 0.025 0.010
ND mg/kg 0.025 0.0050
ND mg/kg 0.050 0.010
ND mg/kg 0.025 0.010
ND mg/kg 0.025 0.0050
ND mg/kg 0.025 0.010
ND mg/kg 0.025 0.010
ND mg/kg 0.025 0.010
ND mg/kg 0.025 0.010
ND mg/kg 0.025 0.010
ND mg/kg 0.025 0.010
ND mg/kg 0.025 0.010
ND mg/kg 0.025 0.0050
ND mg/kg 0.025 0.010
ND mg/kg 0.025 0.010
0.16 mg/kg 0.025 0.010
ND mg/kg 0.025 0.010
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of CALTEST ANALYTICAL LABORATORY
1885 North Kelly Road • Napa, California 94558
(707) 258-4000 • Fax (707) 226-1001 • e-mail: info@caltestlabs.com
06/05/15 02:12 SMS 3755
Analyzed by: AN
05/07 /15 20: 10 VMS 3245 4
05/07/15 20:10 VMS 3245
05/07/15 20:10 VMS 3245
05/07/15 20:10 VMS 3245
05/07/15 20:10 VMS 3245
05/07/15 20:10 VMS 3245
05/07/15 20:10 VMS 3245
05/07/15 20:10 VMS 3245
05/07/15 20:10 VMS 3245
05/07/15 20:10 VMS 3245
05/07 /15 20: 10 VMS 3245
05/07/15 20:10 VMS 3245
05/07 /15 20: 10 VMS 3245
05/07/15 20:10 VMS 3245
05/07/15 20:10 VMS 3245
05/07/15 20:10 VMS 3245
05/07 /15 20: 10 VMS 3245
05/07 /15 20: 10 VMS 3245
05/07 /15 20: 10 VMS 3245
05/07/15 20:10 VMS 3245
05/07 /15 20: 10 VMS 3245
05/07 /15 20: 10 VMS 3245
05/07 /15 20: 10 VMS 3245
05/07/15 20:10 VMS 3245
05/07 /15 20: 10 VMS 3245
05/07/15 20:10 VMS 3245
05/07 /15 20: 10 VMS 3245
05/07/15 20:10 VMS 3245
05/07/15 20:10 VMS 3245
05/07 /15 20: 10 VMS 3245
05/07/15 20:10 VMS 3245
05/07/15 20:10 VMS 3245
05/07 /15 20: 10 VMS 3245
05/07 /15 20: 10 VMS 3245
05/07 /15 20: 10 VMS 3245
05/07 /15 20: 10 VMS 3245
05/07/15 20:10 VMS 3245
05/07 /15 20: 10 VMS 3245
Page 13 of 27
DocuSign Envelope ID: 448F9D83-A76E-4EF1-9A95-3F616E43347D
NELAP/ORELAP Certification 4036
Lab Order: 0050123
Project ID: NPDES QUARTERLY MAY 2015
Solid results are reported on a wet weight basis.
tii ...... Caltest
~II··, 'lot:~ ·1 "·'t}>J .\II. II YI l<",\I I \!!lilt\ 1 lllt\
ENVIRONMENTAL ANAL IL
ANALYTICAL RESULTS
Lab ID Q050123005 Date Collected 5/4/2015 09:35
Sample ID E000767-01 GRIT Date Received 5/5/2015 13:40
CA-ELAP Certification 1664
IIREVJ
Matrix Solid
Results are expressed as wet weight values
Parameters Result Units R. L. MDL DF Prepared Batch Analyzed Batch Qua I
Methylene chloride ND mg/kg 0.15 0.0050 05/07 /15 20: 10 VMS 3245
Naphthalene ND mg/kg 0.025 0.010 05/07/15 20:10 VMS 3245
n-Propylbenzene ND mg/kg 0.025 0.010 05/07 /15 20: 10 VMS 3245
Styrene ND mg/kg 0.025 0.010 05/07/15 20:10 VMS 3245
1, 1, 1,2-Tetrachloroethane ND mg/kg 0.025 0.010 05/07/15 20:10 VMS 3245
1, 1,2,2-Tetrachloroethane ND mg/kg 0.025 0.010 05/07 /15 20: 10 VMS 3245
Tetrachloroethene (PCE) ND mg/kg 0.025 0.010 05/07/15 20:10 VMS 3245
Toluene 4.2 mg/kg 0.005 0.0010 05/12/15 20:00 VMS 3245 6
1,2,3-Trichlorobenzene ND mg/kg 0.025 0.010 05/07/15 20:10 VMS 3245
1,2,4-Trichlorobenzene ND mg/kg 0.025 0.010 05/07/15 20:10 VMS 3245
1, 1,2-Trichloroethane ND mg/kg 0.025 0.0050 05/07/15 20:10 VMS 3245
1, 1, 1-Trichloroethane (TCA) ND mg/kg 0.025 0.010 05/07/15 20:10 VMS 3245
Trichloroethane (TCE) ND mg/kg 0.025 0.010 05/07 /15 20: 10 VMS 3245
Trichlorofluoromethane (F-ND mg/kg 0.025 0.020 05/07 /15 20: 10 VMS 3245
11)
1,2,3-Trichloropropane ND mg/kg 0.025 0.010 05/07 /15 20: 10 VMS 3245
Trichlorotrinuorethane ND mg/kg 0.050 0.010 05/07 /15 20: 10 VMS 3245
(F113)
1,2,4-Trimethylbenzene ND mg/kg 0.025 0.010 05/07/15 20:10 VMS 3245
1,3,5-Trimethylbenzene ND mg/kg 0.025 0.010 05/07 /15 20: 10 VMS 3245
Vinyl chloride ND mg/kg 0.025 0.015 05/07/15 20:10 VMS 3245
Xylenes, total ND mg/kg 0.025 0.0050 05/07/15 20:10 VMS 3245
4-Bromofluorobenzene (SS) 93% 74-130 05/07 /15 20: 10 VMS 3245
Dibromofluoromethane (SS) 103 % 69-129 05/07/15 20:10 VMS 3245
1,2-Dichloroethane-d4 (SS) 95% 61-133 05/07/15 20:10 VMS 3245
Toluene-dB (SS) 93% 71-135 05/07/15 20:10 VMS 3245
Cyanide, Total Analysis Analytical Method: SW846 9012A Analyzed by: BCP
Cyanide 0.25 mg/kg 0.080 0.080 05/09/15 17:05 wco 10778
6/18/2015 16:12 REPORT OF LABORATORY ANALYSIS Page 14 of 27
This report shall not be reproduced, except In full,
without the written consent of CALTEST ANALYTICAL LABORATORY
1885 North Kelly Road• Napa, California 94558
(707) 258-4000 • Fax (707) 226-100 l • e-mail: info@caltestlabs.com
DocuSign Envelope ID: 448F9D83-A76E-4EF1 -9A95-3F616E43347D
NELAP/ORELAP Certification 4036 .. ~-~ .. \, Caltest CA-ELAP Certification 1664
Lab Order: 0050123
Project ID: NPDES QUARTERLY MAY 2015
Analysls Description:
Analysis Method:
METHOD BLANK:
Parameter
Mercury
Mercury Analysis
SW846 7471A
638756
Blank
Result
ND
LABORATORY CONTROL SAMPLE: 638757
Parameter Units
Mercury mg/kg
~ • J I ... ·.:. .... i'; ~ ~ !~ \"\\1)11('\f I \l,lll:\IOH'!
ENVIRONMENTAL ANALYSES
QUALITY CONTROL DATA
Reporting
Limit MDL
0.020 0.0008
Spike
Cone.
0.1
LCS
Result
0.12
QC Batch:
QC Batch Method:
Units Qualifiers
mg/kg
LCS
%Rec
110
%REC
MPR/13565
SW846 7471A
Limits Qualifier
75-125
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 638759 638760
Q050123001 Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Result Result % Rec % Rec Limit RPD
Mercury
Analysis Description:
Analysis Method:
METHOD BLANK:
Parameter
Antimony
Copper
METHOD BLANK:
Parameter
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Lead
Molybdenum
Nickel
Selenium
Silver
Thallium
Vanad ium
Zinc
6/18/2015 16:12
mg/kg 0.0009 0.11 0.115 0.115 108 108 75-125
Metals Analysis by ICP QC Batch:
SW846 60108 QC Batch Method:
638744
Blank Reporting
Result Limit MDL Units Qualifiers
ND 2.0 1.5 mg/kg
ND 2.0 0.2 mg/kg
638744
Blank Reporting
Result Limit MDL Units Qualifiers
ND 2.0 1.0 mg/kg
ND 1.0 0.7 mg/kg
ND 5.0 0.15 mg/kg
ND 0.20 0.05 mg/kg
ND 1.0 0.2 mg/kg
ND 0.4 0.2 mg/kg
ND 1.0 0.5 mg/kg
ND 2.0 1.0 mg/kg
ND 1.0 0.30 mg/kg
ND 2.0 0.8 mg/kg
ND 1.0 0.2 mg/kg
ND 2.0 0.7 mg/kg
ND 0.40 0.20 mg/kg
ND 4.0 1.0 mg/kg
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of CAL TEST ANALYTICAL LABORATORY
1885 North Kelly Road • Napa, California 94558
MPR/13563
SW846 30508
(707) 258-4000 • Fax (707) 226-1001 • e-mail: info@caltestlabs.com
0
Max
RPD Qualifiers
35
Page 15 of 27
DocuSign Envelope ID: 448F9D83-A76E-4EF1-9A95-3F616E43347D
NELAP/ORELAP Certification 4036 CA-ELAP Certification 1664
QUALITY CONTROL DATA
Lab Order: 0050123
Project ID: NPDES QUARTERLY MAY 2015
Analysls Description: Metals Analysis by ICP
Analysls Method: SW846 60108
QC Batch:
QC Batch Method:
MPR/13563
SW846 30508
LABORATORY CONTROL SAMPLE: 638745
Spike LCS LCS %REC
Parameter Units Cone. Result %Rec Limits Qualifier
Antimony mg/kg 20 17 84 75-125
Arsenic mg/kg 20 17 86 75-125
Barium mg/kg 99 90 91 75-125
Beryllium mg/kg 20 19 95 75-125
Cadmium mg/kg 9.9 9.1 92 75-125
Chromium mg/kg 20 18 91 75-125
Cobalt mg/kg 20 17 85 75-125
Copper mg/kg 20 17 88 75-125
Lead mg/kg 99 91 92 75-125
Molybdenum mg/kg 20 16 80 75-125
Nickel mg/kg 20 19 94 75-125
Selenium mg/kg 20 15 77 75-125
Sliver mg/kg 20 19 95 75-125
Thallium mg/kg 99 88 89 75-125
Vanadium mg/kg 20 17 87 75-125
Zinc mg/kg 99 87 88 75-125
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 638747 638748
Q040B96001 Spike MS MSD MS MSD %Rec
Parameter Units Result Cone. Result Result %Rec %Rec Limit RPD
Antimony mg/kg 0 20 15.5 15.4 78 78 75-125 0.6
Arsenic mg/kg 0 20 18.5 18.4 93 93 75-125 0.5
Barium mg/kg 85 100 177 176 92 92 75-125 0.6
Beryllium mg/kg 0 20 18.3 18.1 92 91 75-125 1.1
Cadmium mg/kg 0.43 10 9.31 9.18 89 88 75-125 1.4
Chromium mg/kg 7.3 20 25.2 25.2 90 90 75-125 0
Cobalt mg/kg 0.9 20 17.3 17.2 82 82 75-125 0.6
Copper mg/kg 110 20 121 121 RNC RNC 75-125 0
Lead mg/kg 6 100 95.7 94.5 90 89 75-125 1.3
Molybdenum mg/kg 0 20 17.1 17.3 86 87 75-125 1.2
Nickel mg/kg 6.9 20 25.4 25.3 93 93 75-125 0.4
Selenium mg/kg 1.9 20 16.7 17.4 74 78 75-125 4.1
Silver mg/kg 1.3 20 20.5 20 96 94 75-125 2.5
Thallium mg/kg 0 100 86.5 85.8 87 86 75-125 0.8
Vanadium mg/kg 2 20 19.3 19.1 87 86 75-125
Zinc mg/kg 420 100 509 514 89 95 75-125
6/18/2015 16:12 REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of CAL TEST ANALYTICAL LABORATORY
1885 North Kelly Road• Napa, California 94558
(707) 258-4000 • Fax (707) 226-1001 • e-mail: info@caltestlabs.com
Max
RPD Qualifiers
35
35
35
35
35
35
35
35 7
35
35
35
35 8
35
35
35
35
Page 16 of 27
DocuSign Envelope ID: 448F9D83-A76E-4EF1-9A95-3F616E43347D
NELAP/ORELAP Certification 4036 CA-ELAP Certification 1664
N \I I RON 'I P. TA t NA LY s irs-
QUALITY CONTROL DATA
Lab Order: Q050123
Project ID: NPDES QUARTERLY MAY 2015
Analysls Description: Metals Analysis by ICP, STLC
Analysls Method: SW846 60108 (Leachate)
LEACHATE BLANK: 638765
Blank
Parameter Result
Antimony ND
Arsenic ND
Barium ND
Beryllium ND
Cadmium ND
Chromium ND
Cobalt ND
Copper ND
Lead ND
Molybdenum ND
Nickel ND
Selenium ND
Silver ND
Thallium ND
Vanadium ND
Zinc ND
Reporting
Limit
0.10
0.10
0.15
0.010
0.010
0.10
0.050
0.10
0.10
0.50
0.05
0.50
0.030
0.10
0.02
0.20
MDL
0.040
0.050
0.070
0.0050
0.0040
0.050
0.020
0.030
0.040
0.20
0.02
0.20
0.006
0.040
0.005
0.10
QC Batch:
QC Batch Method:
Units Qualifiers
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg IL
mg/L
MPR/13573
SW846 3010
LABORATORY CONTROL SAMPLE: 639463
Spike LCS LCS %REC
Parameter Units Cone. Result %Rec Limits Qualifier
Antimony mg IL 10 8.9 89 80-120
Arsenic mg/L 2 1.9 94 80-120
Barium mg/L 10 9.6 96 80-120
Beryllium mg/L 2 2 100 80-120
Cadmium mg/L 1 0.96 96 80-120
Chromium mg/L 2 1.9 97 80-120
Cobalt mg IL 2 1.9 95 80-120
Copper mg/L 2 2 99 80-120
Lead mg/L 10 9.7 97 80-120
Molybdenum mg/L 2 1.9 94 80-120
Nickel mg IL 2 2 98 80-120
Selenium mg/L 2 1.6 83 80-120
Silver mg IL 10 9.8 98 80-120
Thallium mg/L 10 9.4 94 80-120
Vanadium mg/L 2 1.9 95 80-120
Zinc mg/L 10 9.1 91 80-120
6/1812015 16:12 REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of CAL TEST ANALYTICAL LABORATORY
1885 North Kelly Road• Napa, California 94558
(707) 258-4000 • Fax (707) 226-1001 • e-mail: info@caltestlabs.com
Page 17 of 27
DocuSign Envelope ID: 448F9D83-A76E-4EF1 -9A95-3F61 6E43347D
NELAP/ORELAP Certification 4036
KNV I RD"N MENTAL _A_N_A LY SES
QUALITY CONTROL DATA
Lab Order: 0050123
Project ID: NPDES QUARTERLY MAY 2015
Analysls Description: Metals Analysis by ICP, STLC QC Batch:
Analysis Method: SW846 60108 (Leachate) QC Batch Method:
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 639465 639466
Parameter
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Lead
Molybdenum
Nickel
Selenium
Silver
Thallium
Vanadium
Zinc
Analysis Description:
Analysis Method:
LEACHATE BLANK:
Parameter
Mercury
Analysis Description:
Analysis Method:
LEACHATE BLANK:
Parameter
Mercury
6/18/2015 16:12
Q050123002 Spike MS
Units Result Cone. Result
mg/L 0.33 10 9.16
mg/L 0.34 2 2.26
mg/L 16 10 25.7
mg/L 0 2 1.89
mg/L 0.014 0.935
mg/L 0.24 2 2.11
mg/L 0.24 2 2.08
mg/L 40 2 42.2
mg/L 0.19 10 9.65
mg/L 2.4 2 4.31
mg/L 0.68 2 2.47
mg/L 0.2 2 1.97
mg/L 0 10 9.72
mg/L 0.074 10 9.51
mg/L 2.8 2 4.63
mg/L 31 10 39.9
Mercury Analysis, STLC, Low Level
SW846 7470A Low Level
638765
Blank
Result
ND
Mercury Analysis, STLC
SW846 7470A
638765
Blank
Result
ND
Reporting
Limit MDL
0.50 0.30
Reporting
Limit MDL
0.50 0.30
MSD MS MSD
Result %Rec %Rec
9.29 88 90
2.33 96 100
25.9 97 99
1.91 95 96
0.941 92 93
2.11 94 94
2.1 92 93
42.6 110 RNC
9.71 95 95
4.36 96 98
2.5 90 91
2.01 89 91
10 97 100
9.65 94 96
4.66 92 93
39.9 89 89
QC Batch:
QC Batch Method:
Units Qualifiers
ug/L
QC Batch:
QC Batch Method:
Units Qualifiers
ug/L
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
without the written consent of CAL TEST ANALYTICAL LABORATORY
1885 North Kelly Road • Napa, California 94558
CA-ELAP Certification 1664
MPR/13573
SW846 3010
%Rec Max
Limit RPD RPO Qualifiers
80-120 1.4 20
80-120 3.1 20
80-120 0.8 20
80-120 1.1 20
80-120 0.6 20
80-120 0 20
80-120 1 20
80-120 0.9 20 7
80-120 0.6 20
80-120 1.2 20
80-120 1.2 20
80-120 2 20
80-120 2.8 20
80-120 1.5 20
80-120 0.6 20
80-120 0 20
MPR/13577
SW846 7470A Low Level
MPR/13577
SW846 7470A
Page 18 of 27
(707) 258-4000 • Fax (707) 226-1001 • e-mail: info@caltestlabs.com
DocuSign Envelope ID: 448F9D83-A76E-4EF1-9A95-3F616E43347D
NELAP/ORELAP Certification 4036
Lab Order: 0050123
Project ID: NPDES QUARTERLY MAY 2015
Analysls Description:
Analysts Method:
Semivolatile Organic Analysis
SW846 8270C
METHOD BLANK:
Parameter
Acenaphthene
Acenaphthylene
Aniline
Anthracene
Benzidine
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b )fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic acid
Benzyl alcohol
Benzyl butyl phthalate
4-Bromophenyl phenyl ether
Carbazole
4-Chloroaniline
bis(2-Chloroethoxy) methane
bis(2-Chloroethyl) ether
bis(2-Chloroisopropyl) ether
4-Chloro-3-methylphenol
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenyl phenyl ether
Chrysene
Total Cresol
Dibenzo(a,h)anthracene
Dibenzofuran
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3'-Dichlorobenzidine
2,4-Dichlorophenol
Dlethylphthalate
2,4-Dimethylphenol
Dimethylphthalate
Di-n-butylphthalate
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphthalate
1,2Diphenylhydrazine/Azobenzen
bis(2-Ethylhexyl) phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
638878
Blank
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
fE\'j 'lf' , I
,I• c <··· '~-i··. ··~s ,,['-, ,, ~ '}), ,.; ~1i '.":r ~ 1.,c... !.< ·1-•· V,;!t,.,,·. ,g, .,,_,, ti., --,J .. , ., I ~ _,. •• IJ \\,'\I \'11( , I I \[',! )I, \ 11 II,~ ...
ENVJRONM~NTAi. A·N ,\LV RS
QUALITY CONTROL DATA
QC Batch:
QC Batch Method:
Reporting
Limit MDL Units Qualifiers
0.33 0.20 mg/kg
0.33 0.20 mg/kg
0.33 0.20 mg/kg
0.33 0.10 mg/kg
0.67 0.50 mg/kg
0.33 0.10 mg/kg
0.33 0.10 mg/kg
0.33 0.10 mg/kg
0.33 0.10 mg/kg
0.33 0.10 mg/kg
2.0 2.0 mg/kg
0.33 0.20 mg/kg
0.33 0.10 mg/kg
0.33 0.20 mg/kg
0.33 0.10 mg/kg
0.33 0.20 mg/kg
0.33 0.20 mg/kg
0.33 0.20 mg/kg
0.33 0.20 mg/kg
0.33 0.30 mg/kg
0.33 0.20 mg/kg
0.33 0.30 mg/kg
0.33 0.20 mg/kg
0.33 0.10 mg/kg
0.67 0.60 mg/kg
0.33 0.10 mg/kg
0.33 0.20 mg/kg
0.33 0.20 mg/kg
0.33 0.20 mg/kg
0.33 0.20 mg/kg
0.33 0.30 mg/kg
0.33 0.30 mg/kg
0.33 0.20 mg/kg
0.33 0.30 mg/kg
0.33 0.20 mg/kg
0.33 0.10 mg/kg
0.33 0.20 mg/kg
0.33 0.20 mg/kg
0.33 0.20 mg/kg
0.33 0.10 mg/kg
0.33 0.20 mg/kg
0.33 0.30 mg/kg
0.33 0.10 mg/kg
0.33 0.20 mg/kg
0.33 0.10 mg/kg
6/18/2015 16:12 REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of CALTEST ANALYTICAL LABORATORY
1885 North Kelly Road• Napa, California 94558
CA-ELAP Certification 1664
SPR/6939
SW846 3540
EVlSEDII
Page 19 of 27
(707) 258-4000 • Fax (707) 226-1001 • e-mail: info@caltestlabs.com
DocuSign Envelope ID: 448F9D83-A76E-4EF1-9A95-3F616E43347D
NELAP/ORELAP Certification 4036 CA-ELAP Certification 1664
Lab Order: 0050123
Project ID: NPDES QUARTERLY MAY 2015
Analysis Description:
Analysis Method:
Semivolatile Organic Analysis
SWB46 8270C
QUALITY CONTROL DATA
QC Batch:
QC Batch Method:
Blank Reporting
Parameter Result Limit MDL Units Qualifiers
Hexachlorobutadiene ND 0.33 0.20 mg/kg
Hexachlorocyclo pentadiene ND 0.33 0.10 mg/kg
Hexachloroethane ND 0.33 0.20 mg/kg
lndeno(1,2,3-cd)pyrene ND 0.33 0.10 mg/kg
lsophorone ND 0.33 0.20 mg/kg
2-Methyl-4,6-dlnitrophenol ND 0.33 0.20 mg/kg
2-Methylnaphthalene ND 0.33 0.20 mg/kg
2-Methylphenol (o-Cresol) ND 0.33 0.30 mg/kg
3 & 4-Methylphenol(m&p Cresol) ND 0.33 0.30 mg/kg
Naphthalene ND 0.33 0.20 mg/kg
2-Nitroaniline ND 0.33 0.20 mg/kg
3-Nitroaniline ND 0.33 0.20 mg/kg
4-Nitroaniline ND 0.33 0.10 mg/kg
Nitrobenzene ND 0.33 0.20 mg/kg
2-Nitrophenol ND 0.33 0.30 mg/kg
4-Nitrophenol ND 0.33 0.20 mg/kg
N-Nitrosodimethylamine ND 0.33 0.20 mg/kg
N-Nitroso-di-n-propylamine ND 0.33 0.20 mg/kg
N-Nitrosodiphenylamine ND 0.33 0.20 mg/kg
Pentachlorophenol ND 0.33 0.20 mg/kg
Phenanthrene ND 0.33 0.20 mg/kg
Phenol ND 0.33 0.20 mg/kg
Pyrene ND 0.33 0.10 mg/kg
Pyridine ND 0.33 0.20 mg/kg
1,2,4-Trichlorobenzene ND 0.33 0.20 mg/kg
2,4,5-Trichlorophenol ND 0.33 0.30 mg/kg
2,4,6-Trichlorophenol ND 0.33 0.30 mg/kg
2-Fluorobiphenyl (SS) 98 10-149 %
2-Fluorophenol (SS) 93 47-105 %
Nitrobenzene-d5 (SS) 83 57-108 %
Phenol-d6 (SS) 95 58-97 %
Terphenyl-d14 (SS) 110 32-120 %
2,4,6-Tribromophenol (SS) 135 26-143 %
LABORATORY CONTROL SAMPLE & LCSO: 638879 638880
Spike LCS LCSO LCS LCSD
Parameter Units Cone. Result Result %Rec %Rec
Acenaphthene mg/kg 3.3 3.46 3.2 104 96
4-Chloro-3-methylphenol mg/kg 6.7 6.36 6.25 95 94
2-Chlorophenol mg/kg 6.7 5.9 5.66 89 85
1,4-Dichlorobenzene mg/kg 3.3 3.22 2.91 97 87
2,4-Dinitrotoluene mg/kg 3.3 3.38 3.15 101 95
4-Nitrophenol mg/kg 6.7 7.18 6.78 108 102
N-Nitroso-di-n-propylamine mg/kg 3.3 2.86 2.62 86 79
6/18/2015 16:12 REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
SPR/6939
SW846 3540
%REC
Limits RPO
67-108 7.8
45-98 1.7
62-106 4.2
55-112 10
56-140 7
67-127 5.7
20-120 8.8
without the written consent of CALTEST ANALYTICAL LABORATORY
1885 North Kelly Road• Napa, California 94558
(707) 258-4000 • Fax (707) 226-100 l • e-mail: info@caltestlabs.com
SEO
Max
RPO Qualifier
68
74
50
50
71
52
50
Page 20 of 27
DocuSign Envelope ID: 448F9D83-A76E-4EF1-9A95-3F616E43347D
NELAP/ORELAP Certification 4036 ,~~, C I \)__ a t est CA-ELAP Ce11ification 1664
, ·~ .-~·.:
'"" \!'\\I) II~ \I I \llt1B\IOH) 1l.'.
ENVIRONMENTAL ANALYSES
QUALITY CONTROL DATA
Lab Order: 0050123
Project ID: NPDES QUARTERLY MAY 2015
Analysis Description: Semivolalile Organic Analysis QC Batch: SPR/6939
Analysis Method: SW846 8270C QC Batch Method: SW846 3540
LABORATORY CONTROL SAMPLE & LCSD: 638879 638880
Spike LCS LCSD LCS LCSD %REC Max
Parameter Units Cone. Result Result % Rec % Rec Limits RPD RPD Qualifier
Pentachlorophenol mg/kg 6.7 9.29 8.74 139 131 53-119 6.1 78 9
Phenol mg/kg 6.7 5.63 5.34 84 80 48-95 5.3 50
Pyrene mg/kg 3.3 3.52 3.35 106 101 53-122 4.9 101
1,2,4-Trichlorobenzene mg/kg 3.3 3.45 3.21 104 96 69-110 7.2 80
2-Fluorobiphenyl (SS) % 102 95 10-149 7.9
2-Fluorophenol (SS) % 90 89 47-105 0.5
Nitrobenzene-d5 (SS) % 95 101 57-108 6.1
Phenol-d6 (SS) % 96 95 58-97 1.6
Terphenyl-d14 (SS) % 118 111 32-120 6.6
2,4,6-Tribromophenol (SS) % 133 137 26-143 3.1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 638881 638882
Q040896001 Spike MS MSD MS MSD %Rec Max
Parameter Units Result Cone. Result Result %Rec %Rec Limit RPD RPD Qualifiers
Acenaphthene mg/kg 0 10 10.9 11 109 110 67-108 0.9 68 11
4-Chloro-3-methylphenol mg/kg 0 20 22.9 23.9 115 120 45-98 4.3 74 11
2-Chlorophenol mg/kg 0 20 18.4 18.6 92 93 62-106 1.1 50
1,4-Dichlorobenzene mg/kg 0 10 8.82 8.7 88 87 55-112 1.4 50
2,4-Dinitrotoluene mg/kg 0 10 11 11 110 110 56-140 0 71
4-Nitrophenol mg/kg 0 20 24.7 27.3 124 137 67-127 10 52 11
N-Nitroso-di-n-propylamine mg/kg 0 10 10.8 11 .6 108 116 20-120 7.1 50
Pentachlorophenol mg/kg 0 20 29.5 27.8 148 139 53-119 5.9 78 12
Phenol mg/kg 41 20 63.5 69.8 113 144 48-95 9.5 50 11
Pyrene mg/kg 0 10 24.1 27.7 241 277 53-122 14 101 11
1,2,4-Trichlorobenzene mg/kg 0 10 10.2 9.64 102 96 69-110 5.6 80
2-Fluorobiphenyl (SS) % 113 110 10-149 2.3
2-Fluorophenol (SS) % 81 104 47-105 25
Nitrobenzene-d5 (SS) % 92 94 57-108 1.8
Phenol-d6 (SS) % 109 116 58-97 5.9 10
Terphenyl-d14 (SS) % 201 241 32-120 18 10
2,4,6-Tribromophenol (SS) % 143 143 26-143 0.1
Analysis Description: Total Extractable Petroleum Hydrocarbon QC Batch: SPR/6946
Analysis Method: SW846 8015(MOD) QC Batch Method: SW846 3541
METHOD BLANK: 639585
Blank Reporting
Parameter Result Limit MDL Units Qualifiers
Diesel Fuel ND 4 2 mg/kg
TPH quantitated as Diesel Fuel ND 4 2 mg/kg
6/18/2015 16:12 REPORT OF LABORATORY ANALYSIS Page 21 of 27
This report shall not be reproduced, except in full,
without the written consent of CALTEST ANALYTICAL LABORATORY
1885 North Kelly Road • Napa, California 94558
(707) 258-4000 • Fax (707) 226-1001 • e-mail: info@caltestlabs.com
DocuSign Envelope ID: 448F9D83-A76E-4EF1-9A95-3F616E43347D
NELAP/ORELAP Certification 4036 (' ';, ~;(f .. ) CaJtest CA-ELAP Ce1iification 1664
Lab Order: 0050123
Project ID: NPDES QUARTERLY MAY 2015
Analysls Description:
' • I ''t • ,:·~'t,.~-\
·1 : .. •JJ \:-.,; \I )"I I{' \I I \I;( )I{\ I (lit\
ENVIRONMENTAL ANALYSES
QUALITY CONTROL DATA
QC Batch:
Analysis Method:
Total Extractable Petroleum Hydrocarbon
SW846 8015(MOD) QC Batch Method:
SPR/6946
SW846 3541
Parameter
o-Terphenyl (SS)
LABORATORY CONTROL SAMPLE:
Parameter
Diesel Fuel
o-Terphenyi (SS)
Blank
Result
92
639586
Units
mg/kg
%
Reporting
Limit MDL
40-139
Spike
Cone.
67
LCS
Result
57
Units Qualifiers
%
LCS
% Rec
85
89
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 639588 639589
Q050228001 Spike MS MSD MS
%REC
Limits Qualifier
36-120
40-139
MSD %Rec
Parameter Units Result Cone. Result Result %Rec %Rec Limit RPD
TPH quantitated as Diesel Fuel mg/kg 1170 200 1820 1620 RNC RNC 28-156 12
o-Terphenyi (SS) % 123 112 40-139 9.4
Analysis Description: Volatile Organic Analysis QC Batch: VMS/3245
Analysis Method: SW846 50308/82608 QC Batch Method: SW846 50308/82608
METHOD BLANK: 638856
Blank Reporting
Parameter Result Limit MDL Units Qualifiers
Benzene ND 0.005 0.002 mg/kg
Bromobenzene ND 0.005 0.002 mg/kg
Bromochloromethane ND 0.005 0.003 mg/kg
Bromodichloromethane ND 0.005 0.002 mg/kg
Bromoform ND 0.005 0.001 mg/kg
Bromomethane (Methyl Bromide) ND 0.020 0.004 mg/kg
n-Butylbenzene ND 0.005 0.002 mg/kg
sec-Butylbenzene ND 0.005 0.002 mg/kg
tert-Butylbenzene ND 0.005 0.002 mg/kg
Carbon tetrachloride ND 0.005 0.002 mg/kg
Chlorobenzene ND 0.005 0.002 mg/kg
Chloroethane (Ethyl Chloride) ND 0.020 0.003 mg/kg
Chloroform ND 0.005 0.002 mg/kg
Chloromethane(Methyl Chloride) ND 0.020 0.002 mg/kg
2-Chlorotoluene ND 0.005 0.002 mg/kg
4-Chlorotoluene ND 0.005 0.002 mg/kg
Dibromochloromethane ND 0.005 0.001 mg/kg
1,2-Dibromo-3-chloropropane ND 0.005 0.002 mg/kg
1,2-Dibromoethane (EDB) ND 0.005 0.001 mg/kg
Dibromomethane ND 0.005 0.002 mg/kg
6/18/2015 16:12 REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of CAL TEST ANALYTICAL LABORATORY
1885 North Kelly Road • Napa, California 94558
(707) 258-4000 • Fax (707) 226-1001 • e-mail: info@caltestlabs.com
Max
RPD Qualifiers
40 7
Page 22 of 27
DocuSign Envelope ID: 448F9D83-A76E-4EF1-9A95-3F616E43347D
NELAP/ORELAP Certification 4036 CA-ELAP Certification 1664
·N ur -Nl'if ,N l\fAL g.
QUALITY CONTROL DATA
Lab Order: 0050123
Project ID: NPDES QUARTERLY MAY 2015
Analysis Description: Volatile Organic Analysis QC Batch: VMS/3245
Analysis Method: SW846 50308/82608 QC Batch Method: SW846 50308/82608
Blank Reporting
Parameter Result Limit MDL Units Qualifiers
1,2-Dichlorobenzene ND 0.005 0.002 mg/kg
1,3-Dichlorobenzene ND 0.005 0.002 mg/kg
1,4-Dichlorobenzene ND 0.005 0.001 mg/kg
Dichlorodifiuoromethane (F-12) ND 0.010 0.002 mg/kg
1, 1-Dichloroethane ND 0.005 0.002 mg/kg
1,2-Dichloroethane (EDC) ND 0.005 0.001 mg/kg
1, 1-Dichloroethene ND 0.005 0.002 mg/kg
cis-1,2-Dichloroethene ND 0.005 0.002 mg/kg
trans-1,2-Dichloroethene ND 0.005 0.002 mg/kg
1,2-Dichloropropane ND 0.005 0.002 mg/kg
1,3-Dichloropropane ND 0.005 0.002 mg/kg
2,2-Dichloropropane ND 0.005 0.002 mg/kg
1, 1-Dichloropropene ND 0.005 0.002 mg/kg
Dichlorotrifluoroethane (F123) ND 0.005 0.001 mg/kg
Ethylbenzene ND 0.005 0.002 mg/kg
Hexachlorobutadiene ND 0.005 0.002 mg/kg
4-lsopropyltoluene ND 0.005 0.002 mg/kg
Methyl tert-butyl ether (MT8E) ND 0.005 0.002 mg/kg
Methylene chloride ND 0.030 0.001 mg/kg
Naphthalene ND 0.005 0.002 mg/kg
n-Propylbenzene ND 0.005 0.002 mg/kg
Styrene ND 0.005 0.002 mg/kg
1, 1, 1,2-Tetrachloroethane ND 0.005 0.002 mg/kg
1, 1,2,2-Tetrachloroethane ND 0.005 0.002 mg/kg
Tetrachloroethene (PCE) ND 0.005 0.002 mg/kg
Toluene ND 0.005 0.001 mg/kg
1,2,3-Trichlorobenzene ND 0.005 0.002 mg/kg
1,2,4-Trichlorobenzene ND 0.005 0.002 mg/kg
1, 1,2-Trichloroethane ND 0.005 0.001 mg/kg
1, 1, 1-Trichloroethane (TCA) ND 0.005 0.002 mg/kg
Trichloroethane (TCE) ND 0.005 0.002 mg/kg
Trichlorofluoromethane (F-11) ND 0.005 0.004 mg/kg
1,2,3-Trichloropropane ND 0.005 0.002 mg/kg
Trichlorotrifiuorethane (F113) ND 0.010 0.002 mg/kg
1,2,4-Trimethylbenzene ND 0.005 0.002 mg/kg
1,3,5-Trimethylbenzene ND 0.005 0.002 mg/kg
Vinyl chloride ND 0.005 0.003 mg/kg
Xylenes, total ND 0.005 0.001 mg/kg
4-8romofiuorobenzene (SS) 89 74-130 %
Dibromofluoromethane (SS) 101 69-129 %
1,2-Dichloroethane-d4 (SS) 90 61-133 %
Toluene-dB (SS) 101 71-135 %
6/18/2015 16:12 REPORT OF LABORATORY ANALYSIS Page 23 of 27
This report shall not be reproduced, except in full,
without the written consent of CALTEST ANALYTICAL LABORATORY
1885 North Kelly Road• Napa, California 94558
(707) 258-4000 • Fax (707) 226-1001 • e-mail: info@caltestlabs.com
DocuSign Envelope ID: 448F9D83-A76E-4EF1-9A95-3F616E43347D
NELAP/ORELAP Certification 4036 CA-ELAP Ce1iification 1664
EN \I I fl ON M £ N 'I' AL AN A LY SES IIREVlSEDII
QUALITY CONTROL DATA
Lab Order: 0050123
Project ID: NPDES QUARTERLY MAY 2015
Analysis Description: Volatile Organic Analysis QC Batch: VMS/3245
Analysis Method: SW846 50308/82608 QC Batch Method: SW846 50308/82608
LABORATORY CONTROL SAMPLE & LCSD: 638857 638858
Spike LCS LCSD LCS LCSD %REC Max
Parameter Units Cone. Result Result %Rec %Rec Limits RPO RPO Qualifier
Benzene mg/kg 0.04 0.0443 0.0366 111 92 50-150 19 50
Bromochloromethane mg/kg 0.04 0.043 0.0365 108 91 50-150 16 50
Bromodichloromethane mg/kg 0.04 0.0452 0.0385 113 96 50-150 16 50
Chlorobenzene mg/kg 0.04 0.0418 0.0343 105 86 50-150 20 50
1, 1-Dichloroethene mg/kg 0.04 0.0444 0.0358 111 90 50-150 21 50
Methyl tert-butyl ether (MTBE) mg/kg 0.04 0.0488 0.0421 122 105 50-150 15 50
Toluene mg/kg 0.04 0.0413 0.0339 103 85 50-150 20 50
Trichloroethane (TCE) mg/kg 0.04 0.0442 0.0371 111 93 50-150 17 50
4-Bromofluorobenzene (SS) % 94 91 74-130 3.2
Dibromofluoromethane (SS) % 100 100 69-129 0
1,2-Dichloroethane-d4 (SS) % 101 98 61-133 3.3
Toluene-dB (SS) % 100 101 71-135 1.2
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 639382 639383
Q050214001 Spike MS MSD MS MSD %Rec Max
Parameter Units Result Cone. Result Result %Rec %Rec Limit RPO RPO Qualifiers
Benzene mg/kg 0 0.2 0.142 0.154 71 77 50-150 8.1 50
Bromochloromethane mg/kg 0 0.2 0.137 0.146 69 73 50-150 6.4 50
Bromodichloromethane mg/kg 0 0.2 0.104 0.0867 52 43 50-150 18 50 13
Chlorobenzene mg/kg 0 0.2 0.111 0.109 56 55 50-150 1.8 50
1, 1-Dichloroethene mg/kg 0 0.2 0.148 0.173 74 87 50-150 16 50
Methyl tart-butyl ether (MTBE) mg/kg 0 0.2 0.163 0.167 82 84 50-150 2.4 50
Toluene mg/kg 0.082 0.2 0.218 0.234 68 76 50-150 7.1 50
Trichloroethene (TCE) mg/kg 0 0.2 0.129 0.135 65 68 50-150 4.5 50
4-8romofluorobenzene (SS) % 92 91 74-130 1.3
Dibromofluoromethane (SS) % 100 109 69-129 8.2
1,2-Dichloroethane-d4 (SS) % 105 112 61-133 6.2
Toluene-dB (SS) % 102 97 71-135 5.5
Analysis Description: Cyanide, Total Analysis QC Batch: WC0/10778
Analysis Method: SW846 9012A QC Batch Method: SW8469012A
METHOD BLANK: 639384
Blank Reporting
Parameter Result Limit MDL Units Qualifiers
Cyanide ND 0.080 0.080 mg/kg
6/18/2015 16:12 REPORT OF LABORATORY ANALYSIS Page 24 of 27
This report shall not be reproduced, except in full,
without the written consent of CALTEST ANALYTICAL LABORATORY
1885 North Kelly Road• Napa, California 94558
(707) 258-4000 • Fax (707) 226-1001 • e-mail: info@caltestlabs.com
DocuSign Envelope ID: 448F9D83-A76E-4EF1-9A95-3F616E43347D
NELAP/ORELAP Certification 4036 CA-ELAP Cettification 1664
EN V JR ON MENTAL AN ALY SES
QUALITY CONTROL DATA
Lab Order: 0050123
Project ID: NPDES QUARTERLY MAY 2015
Analysls Description:
Analysis Method:
Cyanide, Total Analysis
SW846 9012A
QC Batch:
QC Batch Method:
WC0/10778
SW846 9012A
LABORATORY CONTROL SAMPLE: 639385
Parameter
Cyanide
Units
mg/kg
Spike
Cone.
0.3
LCS
Result
0.3
LCS
%Rec
101
%REC
Limits Qualifier
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 639386 639387
Parameter
Cyanide
Analysis Description:
Analysis Method:
METHOD BLANK:
Parameter
Solids, Percent
SAMPLE DUPLICATE:
Parameter
Solids, Percent
6/18/2015 16:12
Q050123001
Units Result
mg/kg 0.69
Spike MS MSD MS MSD % Rec
Cone. Result Result % Rec % Rec Limit
0.6 1.08 1.12 65 72 70-130
RPD
3.6
Percent Solids Analysis
SM20-2540 G
QC Batch:
QC Batch Method:
WGR/5763
SM20-2540 G
639023
Blank
Result
ND
639038
Reporting
Limit MDL Units Qualifiers
0.1 0.1 %
Max
Units
Q050089001
Result
DUP
Result RPD RPD Qualifiers
% 17.8 17.7 0.6 20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of CAL TEST ANAL YT/CAL LABORATORY
1885 North Kelly Road• Napa, California 94558
(707) 258-4000 • Fax (707) 226-1001 • e-mail: info@caltestlabs.com
Max
RPD Qualifiers
30 8
Page 25 of 27
DocuSign Envelope ID: 446F9D63-A76E-4EF1-9A95-3F616E43347D
NELAP/ORELAP Certification 4036 i"iJ C I ~-\r~:·. a test CA-ELAP Certification 1664
·H·bir, '· "W._} \:'\l'\l,tll"\I L\HOllAIOH\'
II
QUALITY CONTROL DATA QUALIFIERS
Lab Order: 0050123
Project ID: NPDES QUARTERLY MAY 2015
QUALITY CONTROL PARAMETER QUALIFIERS
Results Qualifiers: Report fields may contain codes and non-numeric data correlating to one or more of the following
definitions:
NS -means not spiked and will not have recoveries reported for Analyte Spike Amounts
QC Codes Keys: These descriptors are used to help identify the specific QC samples and clarify the report.
MB -Method Blank
Method Blanks are reported to the same Method Detection Limits (MDLs) or Reporting Limits (RLs) as the analytical
samples in the corresponding QC batch.
LCS/LCSD -Laboratory Control Spike I Laboratory Control Spike Duplicate
DUP -Duplicate of Original Sample Matrix
MS/MSD -Matrix Spike I Matrix Spike Duplicate
RPD -Relative Percent Difference
%Recovery -Spike Recovery stated as a percentage
3 Sample diluted due to a high concentration of non-target analyte(s), resulting in increased reporting limits.
7 RNC = Recovery Not Calculated. Matrix Spike/Matrix Spike Duplicate (MS/MSD) recoveries were not calculated due
to the high native concentration in the sample selected for MS/MSD versus the laboratory spike concentration.
6 Low Matrix Spike recovery(ies) due to possible matrix interferences in the QC sample. QC batch accepted based on
LCS and RPD results.
9 Spike recovery for this compound was high, outside Caltest acceptance criteria. A sample result of 'ND' for this
compound should be considered valld, otherwise any other value reported should be considered estimated.
10 Due to matrix interferences present in the sample, surrogate recoveries failed to meet the QA/QC acceptance criteria.
11 Matrix Spike recovery(ies) outside control limits: LCS(LCSD) recoveries and RPD are in control. Possible Matrix
interference in QC sample.
12 Matrix Spike recovery(ies) outside control limits, RPD recovery is in control. Possible Matrix interference in QC
sample.
13 Matrix Spike recovery(ies) outside of control limits. Sample result accepted based on LCS, RPD and Method Blank.
6/16/2015 16:12 REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of CALTEST ANALYTICAL LABORATORY
1885 North Kelly Road• Napa, California 94558
(707) 258-4000 • Fax (707) 226-l001 • e-mail: info@caltestlabs.com
Page 26 of 27
DocuSign Envelope ID: 44BF9D83-A76E-4EF1-9A95-3F616E43347D
NELAP/ORELAP Certification 4036 CA-ELAP Certification 1664
--Nvnrrn~r;;nn·.r'FJ;-1:---x-J\l· L ;S-
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Lab Order: 0050123
Project ID: NPDES QUARTERLY MAY 2015
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch
Q050123001 E000764-01 ASH A SW846 7471A MPR/13565 SW846 7471A MHG/4963
Q050123004 E000766·01 BARSCREEN SW846 7471A MPR/13565 SW846 7471A MHG/4963
Q050123005 E000767-01 GRIT SW846 7471A MPR/13565 SW846 7471A MHG/4963
Q050123002 E000763·01 ASH A SWB46 7470A MPR/13577 SW846 7470A MHG/4968
Q050123004 E000766-01 BARSCREEN SW846 7470A Low Level MPR/13577 SW846 7470A Low MHG/4968
Q050123005 E000767-01 GRIT SW846 7470A Low Level MPR/13577 SW846 7470A Low MHG/4968
Q050123001 E000764-01 ASH A SW846 30508 MPR/13563 SW846 60108 MIC/4479
Q050123004 E000766·01 BARSCREEN SW846 30508 MPR/13563 SW846 60108 MIC/4479
Q050123005 E000767-01 GRIT SW846 30508 MPR/13563 SWB46 60108 MIC/4479
Q050123002 E000763-01 ASH A SW846 3010 MPR/13573 SWB46 60108 MIC/4481
Q050123004 E000766·01 BARSCREEN SW846 3010 MPR/13573 SW846 60108 MIC/4481
Q050123005 E000767-01 GRIT SW846 3010 MPR/13573 SW846 60108 MIC/4481
Q050123003 E000765·01 ASH A (per attached report) REF/2065
Q050123004 E000766-01 BARSCREEN (per attached report) REF/2065
Q050123005 E000767-01 GRIT (per attached report) REF/2065
Q050123004 E000766-01 BARSCREEN SW846 3541 SPR/6946 SW846 8015(MOD) SFU1703
Q050123005 E000767-01 GRIT SWB46 3541 SPR/6946 SW846 8015(MOD) SFU1703
Q050123004 E000766-01 BARSCREEN SW846 3540 SPR/6939 SWB46 8270C SMS/3755
Q050123005 E000767-01 GRIT SW846 3540 SPR/6939 SW846 8270C SMS/3755
Q050123004 E000766-01 BARSCREEN SW846 50308/82608 VMS/3245
Q050123005 E000767-01 GRIT SW846 50308/82608 VMS/3245
Q050123001 E000764-01 ASH A SW846 9012A WC0/10778
Q050123004 E000766·01 BARSCREEN SW846 9012A WC0/10778
Q050123005 E000767-01 GRIT SW846 9012A WC0/10778
Q050123001 E000764·01 ASH A SM20-2540 G WGR/5763
6/18/2015 16:12 REPORT OF LABORATORY ANALYSIS Page 27 of 27
This report shall not be reproduced, except In full,
without the written consent of CALTEST ANALYTICAL LABORATORY
1885 North Kelly Road• Napa, California 94558
(707) 258-4000 • Fax (707) 226-1001 • e-mail: info@caltestlabs.com
DocuSign Envelope ID: 448F9D83·A76E-4EF1 ·9A95·3F616E43347D
464 McCormick Streot, San Loandro, CA 94577
Phonelfa,c (510) 895,3675 I (510) 895-3680
. EMSL Order:
CustomerlD:
CustomerPO:
091506686
CALT50
0050123
•
EMSL Analytical, Inc
http://www.EMSl.com santeandrotab@emsl.com ProjectlD:
Attn: Client Services
Caltest Analytical Laboratories, Inc.
1885 North Kelly Road
NAPA, CA 94558
Proiect: 0050123
Phone: (707) 258-4000
Fax: (707) 226-1001
Received: 05/08/15 10:00 AM
Analysis Date: 5/21/2015
Collected: 5/8/2015
Test Report: PLM Analysis of Bulk Samples for Asbestos via EPA 600/R-93/116 Method
with CARB 435 Prep (Milling) Level A for 0.25% Target Analytical Sensitivity
Sample Description
0050123003 E000765-01 ASH A
091506686-0001
0050123004 E000766-01
091506686-0002 BARSCREEN RAGS
0050123005 E00076-01 GRIT
091506686-0003
Analyst(s)
Matthew Batongbacal (3)
Appearance
Brown
Non-Fibrous
Hom eneous
Brown
Fibrous
Hom eneous
Black
Non-Fibrous
Homogeneous
% Fibrous
100.00% Cellulose
Non-Asbestos
% Non-Fibrous
100.00% Non-fibrous (other)
100.00% Non-fibrous (other)
Asbestos
% Type
None Detected
None Detected
None Detected
Chris Dojlidko, Laboratory Manager
or other approved signatory
This report relates only to the samples listed above and may not be reproduced except In full, without EMSL's wrltten approval. This report must not be used by the client to claim product certification,
approval, or endorsemenl by NVLAP, NIST, or any agency of the federal government. EMSL Is not responsible for sample collection activities or method limitations. Some samples may contain asbestos
fibers below the resolution limit of PLM. EMSL recommends that samples reported as none detected or less than the limit of detection undergo additional analysis via TEM.Samples recelwd In good
condition unless otherwise noted.
Samples analyzed by EMSL Analy1lcal, Inc San Leandro, CA
Initial report from 05/21/2015 14:14:17
Test Report PLMPTC-7.25.0 Printed: 5/21/2015 2:14:17 PM THIS IS THE LAST PAGE OF THE REPORT.
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1;ROJECT NAr.lE I PR<JJbCT NU .. BER: '•"· NY••-~
ANALYTICALlABORATORY NPDES Quarterlv May 2016 4615000068
CLIENT: rEPOl<T A TIN:
City of Palo 1Ali:o Samantha Bialorucki ANALYSES REQUESTED
MAILING At>w~S.~ STATE: rw i5 2501 Embari:adero Way, Palo Alto CA 94303 .,
::; "' 1 .. WNG ADORE= ATIN: Cl .s:, :,: a..
-(Please p~ovide data in CWIQS format zip file and PD F's)
., I E. ..,. I-~ z ;,; .r, .;; i' ~ FliONE NUMBER: rA.l( PHONE NUMBER: SAMPLER (PiUNT & SIGN NAi,IE): ~ a.. Jg E ti :,: w ...
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SAMPLE I-u ~ -CALTEST DATE CONTAINER CU ENT COMP. or .. TIME SAMPLED PRESERVATIVE SAMPLE IDENTIFICATION I SITE ...I 0 2 LAB# SAMPI..ED MATRIX" lYPE/ AJIOU~ LAB# GRAB ,...
II) 0 .J I-I-
511(2015 10:00 SL Soz/SJ None E000764--01 ASH A COMP x x x
5/412015 10:00 SL Soz/SJ None E000763-01 ASH A COMP x
5/412015 10:00 SL 8oz/SJ None E000770-01 ASH 1.-.Jf. A COMP x
¥-51412015 7:00 SL Soz/SJ None E000770·01 Sludge Cake A COMP x x
5/4/2015 9:33 SL 1USJ None E000766-01 Barscreen Rags A GRAB x x x x
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LABORD~R" I Qoso ia'3l
TURN-AROUND TIME
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DRUSH
DUE DATE:
REMARKS
TTLC; Quarterly Composite
STLC (mg/L)
Report Dry Wt in mg/Kg to 3 sig figs.
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--• sv VOA ··cONTAINER TYPES: Al =Amberllir. AHL= soo
-----ml Amber, PT= Pini (f'l;lstlc); OT= Quart (Pla3fio); HG
FT QT VOA = Half Gallon (Pli1Stlc); SJ = Soi Jar, !14 = 4= BACT;
~· ----__ __ 8T=~sTube;VOA=40mLVOA,OTC -OlJ'lerT)'!>e
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~A c altest \l"\:il ANALYJJC\L L\BOllATOmr· Sending Laboratory
Caltest Analytical Laboratory
ENVIRONMENTAL ANALYSES 1885 N. Kelly Rd.
Napa, CA 94558
Phone: (707) 258-4000
Fax: (707) 226-1001
Report To: Client Services
Email: pmgr@caltestlabs.com
SUBCONTRACT CHAIN OF CUSTODY
PROJECT ID I PO NUMBER -Q050123
Receiving Laboratory
EMSL Analytical, Inc.
464 Mc Mormick St.
San Leandro, CA 94577
Phone: (510) 895-3675
Fax: (510) 895-3680
Page 1 of 1
PMReview: ~
Due Date: 0.5/22/15 (contact if due date cannot be met)
0050123004 E000766-01 BARSCREEN
RAGS
0050123005 E000767-01 GRIT
~~
Relinquished By
I
Rennqulshed By
Thursday, May 07 2015 12:11PM
. ~··~-:~-":-· ... ~~ ---c~n~Jfl.e! . :!"~ ~~-~ ~ -~;._ .. ::' -t -~~ :.:-.~~rs~~~-::_ i~J;;f.[;:-:
Ma;fri~~SaJ?Jple:l!>~te·· .._._~"TYP!t~. 1;'..l'J!}f~v~tT~e· Rtci.u,~eg_~l]_~lY.~~ ·:.,; _.l .
SL 05/04/2015 10:00 '518c;. Nme:-Asbestos Analysis -PLM CarbA
SL 05/04/2015 09:33 Asbestos Analysis -PLM Carb A
SL 05/04/2015 09:35 L ___k_ Asbestos Analysis -PLM Carb A
5}7hS-;530 ~
Date/Time Received By Date/Time
Date /Time Received By Date I Time
Matrix: AQ -Aqueous OW -Drinking Woter SL -Solid
DocuSign Envelope ID: 448F9D83-A76E-4EF1-9A95-3F616E43347D
--DAVI LABORATORIES, ENVIRONMENTAL ASSOCIATES
730 Alfred Nobel Dr. * Hercules, CA 94547 (510) 724-9450
ANALYTICAL RES UL TS
REPORTS
Company: City of Palo Alto WQCP
Address: 2501 Embarcadero Way
Palo Alto, CA 94303
Contact: Samantha Bialorucki
Project Manager
Date: August 27, 2015
Project Number: NPDES & Non-NPDES, WQCP
TABLE I
Sample ID Sample Matrix EPA Analyses Results +
Date Method pCi/gram
E000766 05-04-15 Solid
BAR SCREEN RAGS (09:33)
Analyses completed on:
8/25/15 900.0 Gross Alpha 0.07 ±
8/25/15 900.0 Gross Beta 0.06 ±
8/11/15 901.1 K-40 ND
8/11/15 901.1 1-131 ND
8/11/15 901.1 Mn-54 ND .
8/11/15 901.1 Co-58 ND
8/11/15 901.1 Co-60 ND
8/11/15 901.1 Cs-137 ND
8/11/15 901.1 Eu-152 ND
8/11/15 901.1 Eu-154 ND
8/11/15 901.1 Eu-155 ND
8/11/15 901.1 lr-192 ND
8/11/15 901.1 Tl-208 ND
8/11/15 901.1 Pb-210 0.02 ±
8/11/15 901.1 Bi-212 ND
8/11/15 901.1 Pb-212 ND
8/11/15 901.1 Bi-214 ND
8/11/15 901.1 Pb-214 ND
8/11/15 901.1 Ra-226 ND
8/11/15 901.1 Ac-228 ND
8/11/15 901.1 Th-228 ND
8/11/15 901.1 Th-230 ND
8/11/15 901.1 Th-232 ND
8/11/15 901.1 Th-234 0.03 ±
8/11/15 901.1 Pa-234m ND
8/11/15 901.1 U-233/234 ND
8/11/15 901.1 U-235 ND
8/11/15 901.1 U-238 ND
2 sigma MDA
Error
0.03 0.01
0.03 0.05
0.02 0.25
0.01 0.30
0.01 0.01
0.01 0.01
0.01 0.01
0.01 0.01
0.01 0.01
0.01 0.02
0.01 0.01
0.01 0.01
0.01 0.04
0.02 0.02
0.03 0.08
0.01 0.01
0.01 0.02
0.01 0.02
0.01 0.03
0.01 0.03
0.01 0.03
0.01 0.20
0.01 0.02
0.01 0.03
0.01 0.01
0.01 0.02
0.01 0.01
0.01 0.02
DocuSign Envelope ID: 448F9D83-A76E-4EF1-9A95-3F616E43347D
TABLE I (cont'd)
Sample-ID Sample· MatFiX-EPA-Analyses Re-suits +-2-sigma MDA
Date Method ~Ci/gram Error
E000767 05-04-15 Solid
GRIT (09:35)
Analyses completed on:
8/25/15 900.0 Gross Alpha 1.62 ± 1.30 0.62
8/25/15 900.0 Gross Beta ND 2.70 3.78
8/12/15 901.1 K-40 0.33 ± 0.04 0.20
8/12/15 901.1 I-131 ND 0.01 0.10
8/12/15 901.1 Mn-54 ND 0.01 0.01
8/12/15 901.1 Co-58 ND 0.01 0.01
8/12/15 901.1 Co-60 ND 0.01 0.01
8/12/15 901.1 Cs-137 ND 0.01 0.01
8/12/15 901.1 Eu-152 ND 0.01 0.01
8/12/15 901.1 Eu-154 ND 0.01 0.02
8/12/15 901.1 Eu-155 ND 0.01 0.01
8/12/15 901.1 Ir-192 ND 0.01 0.01
8/12/15 901.1 Tl-208 ND 0.01 0.04
8/12/15 901.1 Pb-210 0.06 ± 0.01 0.01
8/12/15 901.1 Bi-212 ND 0.01 0.07
8/12/15 901.1 Pb-212 ND 0.01 0.01
8/12/15 901.1 Bi-214 ND 0.01 0.12
8/12/15 901.1 Pb-214 ND 0.01 0.02
8/12/15 901.1 Ra-226 0.01 ± 0.01 0.01
8/12/15 901.1 Ac-228 ND 0.01 0.03
8/12/15 901.1 Th-228 ND 0.01 0.04
8/12/15 901.1 Th-230 ND 0.01 0.02
8/12/15 901.1 Th-232 0.02 ± 0.01 0.01
8/12/15 901.1 Th-234 0.05 ± 0.01 0.02
8/12/15 901.1 Pa-234m ND 0.02 0.07
8/12/15 901.1 U-233/234 0.15 ± 0.03 0.01
8/12/15 901.1 U-235 ND 0.01 0.01
8/12/15 901.1 U-238 0.06 ± 0.01 0.01
DocuSign Envelope ID: 448F9D83-A76E-4EF1-9A95-3F616E43347D
TABLE I (cont'd)
-Sample rn -Sample Matrix EPA Analy-ses Results + 2-sigma MDA
Date Method pCi/gram Error
E000770 05-14-15 Solid
SLUDGE CAKE (07:00)
Analyses completed on:
8/25/15 900.0 Gross Alpha 1.48 ± 0.37 0.08
8/25/15 900.0 Gross Beta 1.35 ± 0.32 0.38
6/08/14 901.1 K-40 0.79 ± 0.03 0.27
8/13/15 901.1 I-131 ND 0.05 0.70
8/13/15 901.1 Mn-54 ND 0.01 0.01
8/13/15 901.1 Co-58 ND 0.01 0.01
8/13/15 901.1 Co-60 ND 0.01 0.01
8/13/15 901.1 Cs-137 ND 0.01 0.01
8/13/15 901.1 Eu-152 ND 0.01 0.02
8/13/15 901.1 Eu-154 ND 0.01 0.02
8/13/15 901.1 Eu-155 ND 0.01 0.01
8/13/15 901.1 Ir-192 ND 0.01 0.01
8/13/15 901.1 Tl-208 ND 0.01 0.01
8/13/15 901.1 Pb-210 ND 0.01 0.02
8/13/15 901.1 Bi-212 ND 0.01 0.17
8/13/15 901.1 Pb-212 ND 0.01 0.01
8/13/15 901.1 Bi-214 ND 0.01 0.16
8/13/15 901.1 Pb-214 ND 0.01 0.29
8/13/15 901.1 Ra-226 ND 0.01 0.02
8/13/15 901.1 Ac-228 ND 0.01 0.03
8/13/15 901.1 Th-228 ND 0.02 0.05
8/13/15 901.1 Th-230 ND 0.02 0.14
8/13/15 901.1 Th-232 ND 0.01 0.03
8/13/15 901.1 Th-234 0.10 ± 0.01 0.03
8/13/15 901.1 Pa-234m ND 0.01 0.10
8/13/15 901.1 U-233/234 0.02 ± 0.01 0.02
8/13/15 901.1 U-235 ND 0.01 0.01
8/13/15 901.1 U-238 0.01 ± 0.01 0.01
DocuSign Envelope ID: 448F9D83-A76E-4EF1-9A95-3F616E43347D
Sample ID Sample Matrix EPA Analyses Results ± 2 Sigma MDA
Date Method pCi/gram Error
E000765-01B 04-27-15 Solid
ASH (00:00)
Analyses completed on:
8/25/15 900.0 Gross Alpha 70.74 ± 11.97 1.67
8/25/15 900.0 Gross Beta 56.58 ± 6.79 6.46
8/14/15 901.1 K-40 3.89 ± 0.21 1.64
8/14/15 901.1 Mn-54 ND 0.01 0.07
8/14/15 901.1 Co-58 ND 0.01 0.07
8/14/15 901.1 Co-60 ND 0.01 0.06
8/14/15 901.1 Cs-137 0.15 ± 0.02 0.06
8/14/15 901.1 Eu-152 ND 0.01 0.01
8/14/15 901.1 Eu-154 ND 0.01 0.03
8/14/15 901.1 Eu-155 ND 0.02 0.02
8/14/15 901.1 lr-192 ND 0.01 0.02
8/14/15 901.1 Tl-208 0.01 ± 0.01 0.01
8/14/15 901.1 Pb-210 0.42 ± 0.02 0.10
8/14/15 901.1 Bi-212 2.20 ± 0.19 1.01
8/14/15 901.1 Pb-212 2.44 ± 0.24 0.98
8/14/15 901.1 Bi-214 0.44 ± 0.03 0.11
8/14/15 901.1 Pb-214 0.30 ± 0.02 0.14
8/14/15 901.1 Ra-226 0.43 ± 0.03 0.11
8/14/15 901.1 Ac-228 1.29 ± 0.12 0.69
8/14/15 901.1 Th-228 1.01 ± 0.05 0.32
8/14/15 901.1 Th-230 1.44 ± 0.03 0.16
8/14/15 901.1 Th-232 0.56 ± 0.03 0.09
8/14/15 901.1 Th-234 10.24 ± 0.12 0.18
8/14/15 901.1 Pa-234m 11.57 ± 0.47 0.98
8/14/15 901.1 U-233/234 9.65 ± 0.19 0.25
8/14/15 901.1 U-235 0.37 ± 0.01 0.05
8/14/15 901.1 U-238 10.89 ± 0.12 0.13
DocuSign Envelope ID: 448F9D83-A76E-4EF1-9A95-3F616E43347D
TABLE II QC RESULTS
Sample ID Nuclide
Laboratory Control Sample
LCS
Blank
:Patricia :tJrn
Patricia Davi
QA/QC Manager
Davi Laboratories
Gross Alpha
Gross Beta
Co-60
Cs-137
Ra-226
U-233/234
U-235
U-238
Gross Alpha
Gross Beta
K-40
Mn-54
Co-58
Co-60
Cs-137
Eu-152
Eu-154
Eu-155
Pb-210
Ra-226
Th-230
Th-232
Pa-234m
Bi-212
Pb-212
Bi-214
Pb-214
U-233/234
U-235
U-238
Results ±
pCi/Sample
352.61 ±
587.71 ±
8131.74 ±
5328.58 ±
1131.25 ±
6517.11 ±
316.32 ±
6329.29 ±
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
2 Sigma MDA Amount Evaluation
Error added % Recovery
Ci
3.63 0.75 386.65 91.17
6.17 0.05 604.45 97.23
48.11 0.09 8936.48 90.99
41.62 0.05 5513.26 96.65
9.86 0.07 1243.55 90.97
19.06 5.62 6800.06 95.84
3.10 2.11 340.00 93.03
32.41 16.47 6800.06 93.07
0.09 0.12 NA
0.42 0.91 NA
0.26 1.18 NA
0.01 0.02 NA
0.01 0.02 NA
0.01 0.02 NA
0.01 0.03 NA
0.01 0.02 NA
0.01 0.03 NA
0.01 0.02 NA
0.01 0.06 NA
0.01 0.09 NA
0.03 0.10 NA
0.01 0.10 NA
0.01 0.15 NA
0.01 0.02 NA
0.01 0.09 NA
0.01 0.20 NA
0.02 0.06 NA
0.02 0.07 NA
0.03 0.05 NA
0.01 0.12 NA
DocuSign Envelope ID: 448F9D83-A76E-4EF1-9A95-3F616E43347D
PALO AL TO REGIONAL WATER QUALITY CONTROL PLANT
INCINERATOR ASH REPORT FOR WET SEASON 2015
Sludge dewatering method: Belt filter presses followed by incineration
FEB 2015 INCINERATOR QUARTERLY ASH REPORT
.. ~ ,,.. VrJ
TTL:C STLC -... ... ,· l' -· --; . "" .. ,. , ._, . ·-· ,,·,
Sample Collection Dates: 11/2014-1/2015; Composited 2/2/2015
!Extraction Date: II 2/6-1 0/2015 I Extraction Dates: 2/13-17/2015
Analytes IAnal}'.sis Date: II 2/11-18/2015 IIAnal}'.sis Date: I 2/18/2015
TTLC Max. mg/kg I Method I RL/MDL Limit (mg/kg) (Wet
(mg/kg) Weight)
Antimony 500 2.0 / 1.5 5.4 A
Arsenic 500 2.0 I .99 7.6 A
Barium 10000 1.0 I .69 820 A
Beryllium 75 4.0 I .15 ND A
Cadmium 100 0.20 I .050 1.3 A
Chromium 2500 1.0 I .20 63 A
Cobalt 8000 0.40/ .20 17 A
Copper 2500 4.0 I 0.40 1900 A
Lead 1000 1.0 I 0.50 67 A
Mercury 20 .020 I .00080 DNQ D (.0014)
Molybdenum 3500 2.0 I .99 34 A
Nickel 2000 1.0 / .30 78 A
Selenium 100 2.0 I 0.79 8.2 A
Silver 500 1.0/0.15 18 A
Thallium 700 2.0 I 0.69 2.3 A
Vanadium 2400 0.40 I .20 70 A
Zinc 5000 16/ 4.0 2200 A
Cyanide --0.08/0.08 0.73 E
T.91~t&ciJJcl~:;J!1.-Asb ', ,' METHOD II Analysis Date ,;,._,;, ·,;
100.0% F I 2/9/2015
ND = Not detected at or above the detection limit.
DNQ = Data not quantified, result between MDL and RL
NOTE = All data in the table are based on Quarterly
composites made up of ash from Nov, Dec and Jan.
STLC
Max.
Limit
(mg/L)
15
5
100
0.75
1
560
80
25
5
0.2
350
20
1
5
7
24
250
-
B RLIMDL
(mg/L) Method
.050 I .010 20 B
0.10 I 0.030 44 B
.050 I .020 0.21 B
.0005/.0003 ND c
0.03 / .006 ND B
[Methods A-El Caltest Analytical
[Method F] Palo Alto RWQCP
A= SW846 -30508/601 osl
B= SW846 -3010/60108
C= SW846 -7470A
D =SW846 7471A
E= SW846 9012 A
F= SM 2540G
1 of 1
DocuSign Envelope ID: 448F9D83-A76E-4EF1-9A95-3F616E43347D
PALO AL TO REGIONAL WATER QUALITY CONTROL PLANT
INCINE-RATOR ASH REPORT FO~DRY SEASOt-J 2~1 5
Sludge dewatering method: Belt filter presses followed by incineration
MAY 2015 INCINERATOR QUARTERLY ASH REPORT
•"• . IT.LC r STLC ·. ·:.:~ . ""· ~= --.•: '-' --~-•
Sample Collection Dates: 2/2015-4/2015; Composited 5/4/2015
!Extraction Date: II 5/6/2015 I Extraction Dates: 5/11-12/2015
Analytes IAnal}:'.sis Date: II 5/07-18/2015 l!Anal}:'.sis Date: I 5/13-14/2015
TTLC Max. n. B STLC RUMDL mg 9 Max Limit (mg/kg) (Wet Method LI 't
(mg/kg) Weight) (m;,~)
Antimony 500 2.0 / 1.5 3.5 A 15
Arsenic 500 2.0 I 1.0 4.6 A 5
Barium 10000 1.0 I .70 830 A 100
Beryllium 75 5.0 I .15 ND A 0.75
Cadmium 100 0.20 I .050 0.36 A 1
Chromium 2500 1.0 I .20 70 A 560
Cobalt 8000 0.40/ .20 19 A 80
Copper 2500 4.0 I 0.40 1900 A 25
Lead 1000 1.0 I 0.50 55 A 5
Mercury 20 .020 I .00060 DNQ D 0.2 0.0009
Molybdenum 3500 2.0 I 1.0 29 A 350
Nickel 2000 1.0 I .30 81 A 20
Selenium 100 2.0 I 0.60 7.9 A 1
Silver 500 1.0 I 0.15 14 A 5
Thallium 700 2.0 I 0.70 2.6 A 7
Vanadium 2400 0.40 I .20 77 A 24
Zinc 5000 8.0/ 2.0 2000 A 250
Cyanide -0.08/0.08 0.69 E ---
TQ.J~I $ol!d~cin))J;J;I.:: ): METHOD Analysis Date
100.0o/o F 5/7/2015
ND= Not detected at or above the detection limit.
DNQ = Data not quantified, result between MDL and RL
NOTE = All data in the table are based on Quarterly
composites made up of ash from Feb, March, April.
[:] RLIMDL
(mg/L) Method
.070 I .015 16 B
0.10/0.030 40 B
.10 I .040 0.19 B
.0005/.0003 ND c
0.030 I .0060 ND B
[Methods A-E] Caltest Analytical
[Method F] Palo Alto RWQCP
A= SW846 -30508/601 osl
B= SW846 -3010/601 OB
C= SW846 -7 4 70A
D =SW846 7471A
E= SW846 9012 A
F= SM 2540G
1 of 1
DocuSign Envelope ID : 448F9D83-A76E-4EF1-9A95-3F616E43347D
PALO AL TO REGIONAL WATER QUALITY CONTROL PLANT
INCINERATOR ASH REPORTFOR DRY SEASON2 015
Sludge dewatering method: Belt filter presses followed by incineration
AUG 2015 INCINERATOR QUARTERLY ASH REPORT
.,
TTLC· ' STLC r.r. • -·-· ~
Sample Collection Dates: 5/2015-7/201 5; Composited 8/3/2015
!Extraction Date: II 8/07-13/2015 I Extraction Dates: 8/13/2015
Analytes Analysis Date: 8/11-14/2015 IAnall sis Date: I 8/14-17/2015
TTLC Max. mg/kg STLC [:]Method RL/MDL Max. RL/MDL Limit (mg/kg) (Wet Method Limit (mg/L) (mg/kg) Weight) (mg/L)
Antimony 500 2.0 I 1.5 3.9 A
Arsenic 500 2.0 I 0.99 5.0 A
Barium 10000 1.0 I .69 800 A
Beryllium 75 4.0 I .15 ND A
Cadmium 100 0.20 I .050 2.4 A
Chromium 2500 1.0 I .20 70 A
Cobalt 8000 0.40/ .20 20 A
Copper 2500 4.0 I 0.40 1960 A
Lead 1000 1.0 I 0.50 64 A
Mercury 20 .020 I .00081 0.041 D
Molybdenum 3500 2.0 I 0.99 56 A
Nickel 2000 1.0 I .30 84 A
Selenium 100 2.0 I 0.99 6.3 A
Silver 500 1.0 I 0.15 16 A
Thallium 700 2.0 I 0.69 DNQ 1.6 A
Vanadium 2400 0.40 I .20 63 A
Zinc 5000 16/ 4.0 2800 A
Cyanide ---0.080/0.080 0.44 E
Total Sqlicli·irl:'A:sh , · ,:, METHOD Analysis Date
100.0% F 8/6/2015
ND = Not detected at or above the detection limit.
DNQ = Data not quantified, result between MDL and RL
NOTE = All data in the table are based on Quarterly
composites made up of ash from May, June, and July.
15
5
100
0.75
1
560
80
25
5
0.2
350
20
1
5
7
24
250
---
.15 I .070 19 B
0.10 I 0.030 41 B
.10/ .040 0.27 B
.0005/.0003 ND c
0.03 I .006 ND B
[Methods A-E] Caltest Analytical
[Method F] Palo Alto RWQCP
A= SW846 -30508/601081
B= SW846 -3010/601 OB
C= SW846 -7 4 70A
D =SW846 7471A
E= SW846 9012 A
F= SM 25408
1 of 1
DocuSign Envelope ID: 448F9D83-A76E-4EF1-9A95-3F616E43347D
PALO AL TO REGIONAL WATER QUALITY CONTROL PLANT -----------INC IN ERA TOR ASH REPORT FOR WET SEASON 2015
Sludge dewaterlng method: Belt filter presses followed by incineration
NOV 2015 INCINERATOR QUARTERLY ASH REPORT
IO · . ~.'f;lLO I STLC
Sample Collection Dates: 8/2015-10/2015; Composited 10/26/2015
IPreeare Date: II 11 /17-24/2015 I Prepare Dates: 11/17-19/2015
Analytes IAnallsis Date: II 11 /10-25/2015 IIAnallsis Date: I 11/18-19/2015
ITLC Max. mg/kg STLC B RUMDL Max. RUMDL Limit (mg/kg) (Wet Method Limit (mg/L) Method
(mg/kg) Weight)
Antimony 500 2.0 I 1.5 4.0 A
Arsenic 500 2.0 I 1.0 5.8 A
Barium 10000 1.0 I .69 730 A
Beryllium 75 4.0 I .15 ND A
Cadmium 100 0.20 I .050 0.47 A
Chromium 2500 1.0 I .20 60.4 A
Cobalt 8000 0.40/ .20 17 A
Copper 2500 7.9 I 0.79 2000 A
Lead 1000 1.0 I 0.50 59 A
Mercury 20 .020 I .00080 0.043 D
Molybdenum 3500 2.0 I 0.99 300 A
Nickel 2000 1.0 I .30 77 A
Selenium 100 2.0 I 0.99 4.5 A
Silver 500 1.0 I 0.15 16 A
Thallium 700 2.0 I 0.69 DNQ 0.7 A
Vanadium 2400 0.40 I .20 56 A
Zinc 5000 16/ 4.0 2500 A
Cyanide ---0.080/0.080 0.72 E
Total;.Sollits J11:·.A'sh ~-, . METHOD Analysis Date
100.0% F 11/6/2015
ND = Not detected at or above the detection limit.
DNQ = Data not quantified, result between MDL and RL
NOTE = All data in the table are based on Quarterly
composites made up of ash from August, September, and
October.
(mg/L)
15
5
100
0.75
1
560
80
25
5
0.2
350
20
1
5
7
24
250
---
.15 / .070 12 B
0.10 I 0.030 46 B
.05/ .040 0.07 B
.0005/0.0003 ND c
0.03 I .006 ND B
[Methods A-E] Caltest Anal ytical
[Method F] Palo Alto RWQCP
A= SW846 -30508/601081
B= SW846 -3010/60108
C= SW846 -7470A
D =SW846 7471A
E= SW846 9012 A
F= SM 2540G
()oQj$' n Envol ID: 448F9D93·A76E-4El't·9A95· 816E4334 D
1• •.
I .· '·
EXHIBIT A-2
Ash Bin Cover
[
1 .. ' ,.,
ll
l
I
.
I
I
I
ij
1
" ,')' ,,
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DocuSign Envelope ID: 448F9D83-A76E-4EF1-9A95-3F616E43347D
EXHIBITS
SCHEDULE OF PERFORMANCE
CONTRACTOR shall perform the Services according to the following schedule: Ongoing services for a
period of three(3) years.
Rev. February 22, 2016
DocuSign Envelope ID: 448F9083-A76E-4EF1-9A95-3F616E43347D EXHIBITC
SCHEDULE OF FEES
CITY shall pay CONTRACTOR according to the following rate schedule. The maximum amount of compensation to be paid to CONTRACTOR, including both payment for
services and reimbursable expenses, shall not exceed the amounts set forth in Sections 5 and 6 of the Agreement. Any services provided or hours worked for which
payment would result in a total exceeding the maximum amount of compensation set forth herein shall be at no cost to CITY.
Bid PSC1 Unit PSC1 Lin'e
Item Bid Schedule Section Description UOM Qty Price Total I
A-1 A: ash hauling & disposal Disposal cost of ash TON 723 $65.00 $46,995.00
A-2 A: ash hauling & disposal Transportation cost of ash: LOAD 53 $1,200.00 $63,600.00
A-3 A: ash hauling & disposal Liner installation fee for ash -per load LOAD 53 $50.00 $2,650.qo
A-4 A: ash hauling & disposal Bin Rental for ash DAYS 365 $9.00 $3,285.00
A-5 A: ash hauling & disposal CA Non-RCRA taxes for ash; based on the most current CA BOE schedule TON 723 $23.23 $16,795.29
A-6 A: ash hauling & disposal Local taxes for ash, as necessary, per ton TON 723 $6.50 $4,699.50
A-7 A: ash hauling & disposal Surcharges/fees for ash, lump sum LS 1 $0.00 $0.00
Subtotal $138,024.79
8-1 B: sludge hauling & disposal Disposal cost of sludge TON 150 $22.00 $3,300.00 I
8-2 B: sludge hauling & disposal Transportation cost for sludge LOAD 12 $600.00 $7,200.00
8-3 B: sludge hauling & disposal Liner installation fee for sludge -per load LOAD 12 $50.00 $600.00
8-4 B: sludge hauling & disposal Bin Rental DAYS 12 $9.00 $108.00
8-5 B: sludge hauling & disposal Local taxes, as necessary, per ton TON 150 $0.00 $0.00
8-6 B: sludge hauling & disposal Surcharges/fees for sludge, lump sum LS 1 $0.00 $0.00
8-7 B: sludge hauling & disposal Roll-off bin mobilization during backup sludge hauling service EA 6 $450.00 $2,700.00
Onsite truck and truck driver to move empty and full bins in and out of
8-8 B: sludge hauling & disposal incinerator building during backup sludge handling service HR 481 $95.00 $4,560.<ilO
Subtotal $18,468.00
Contract Year 1, Total for Bid Schedules A and B Subtotal $156,4921.79
Price Increases price increase -Year 2 % 1 3.00% $4,694.78
Price Increases price increase -Year 3 % 1 3.00% $4,835.63
Contract Year 1, Total for Bid Schedules A and B $156,492.79
Contract Year 2, Total for Bid Schedules A and B $161,18~.57
Contract Year 3, Total for Bid Schedules A and B $166,023.20
1 PSC Industrial Outsourcing, LP I 3yTotal
I
$483,703.56
UOM = unit of measurement; Qty= quantity; LS= lump sum; EA= each; HR= hour
DocuSign Envelope ID: 448F9D83-A76E-4EF1-9A95-3F616E43347D
EXHIBITl>
INSURANCE REQUIREMENTS
CONTRACTORS TO THE CITY OF PALO AL TO (CITY), AT THEIR SOLE EXPENSE, SHALL FOR THE TERM
OF THE CONTRACT OBTAIN AND MAINTAIN INSURANCE IN THE AMOUNTS FOR THE COVERAGE
SPECIFIED BELOW, AFFORDED BY COMPANIES WITH AM BEST'S KEY RATING OF A-:VII, OR
HIGHER, LICENSED OR AUTHORIZED TO TRANSACT INSURANCE BUSINESS IN THE STATE OF
CALIFORNIA.
AW ARD IS CONTINGENT ON COMPLIANCE WITH CITY'S INSURANCE REQUIREMENTS, AS SPECIFIED,
BELOW:
MINIMUM LIMITS
REQUIRED TYPE OF COVERAGE REQUIREMENT EACH
YES
YES
YES
YES
NO
YES
OCCURRENCE AGGREGATE
WORKER'S COMPENSATION STATUTORY
EMPLOYER'S LIABILITY STATUTORY
BODILY INJURY $1,000,000 $1 ,000,000
GENERAL LIABILITY, INCLUDING
PERSONAL INJURY, BROAD FORM PROPERTY DAMAGE $1,000,000 $1,000,000
PROPERTY DAMAGE BLANKET
CONTRACTUAL, AND FIRE LEGAL BODILY INJURY & PROPERTY $1,000,000 $1,000,000
LIABILITY DAMAGE COMBINED.
BODILY INJURY $1,000,000 $1,000,000
-EACH PERSON $1,000,000 $1,000,000
AUTOMOBILE LIABILITY, -EACH OCCURRENCE $1,000,000 $1,000,000
INCLUDING ALL OWNED, HIRED, PROPERTY DAMAGE $1,000,000 $1,000,000 NON-OWNED
BODILY INJURY AND PROPERTY $1,000,000 $1,000,000
DAMAGE, COMBINED
PROFESSIONAL LIABILITY,
INCLUDING, ERRORS AND
OMISSIONS, MALPRACTICE (WHEN
APPLICABLE), AND NEGLIGENT
PERFORMANCE ALL DAMAGES $1,000,000
THE CITY OF PALO ALTO IS TO BE NAMED AS AN ADDITIONAL INSURED: CONTRACTOR, AT
ITS SOLE COST AND EXPENSE, SHALL OBTAIN AND MAINTAIN, IN FULL FORCE AND
EFFECT THROUGHOUT THE ENTIRE TERM OF ANY RESULTANT AGREEMENT, THE
INSURANCE COVERAGE HEREIN DESCRIBED, INSURING NOT ONLY CONTRACTOR AND
ITS SUBCONSULTANTS, IF ANY, BUT ALSO, WITH THE EXCEPTION OF WORKERS'
COMPENSATION, EMPLOYER'S LIABILITY AND PROFESSIONAL INSURANCE, NAMING AS
ADDITIONAL INSUREDS CITY, ITS COUNCIL MEMBERS, OFFICERS, AGENTS, AND EMPLOYEES.
I. INSURANCE COVERAGE MUST INCLUDE:
A. A PROVISION FOR A WRITTEN THlRTY DAY ADVANCE NOTICE TO CITY OF CHANGE
IN COVERAGE OR OF COVERAGE CANCELLATION; AND
B. A CONTRACTUAL LIABILITY ENDORSEMENT PROVIDING INSURANCE COVERAGE
FOR CONTRACTOR'S AGREEMENT TO INDEMNIFY CITY.
C. DEDUCTIBLE AMOUNTS IN EXCESS OF $5,000 REQUIRE CITY'S PRIOR APPROVAL.
II. CONT ACTOR MUST SUBMIT CERTIFICATES(S) OF INSURANCE EVIDENCING REQUIRED
COVERAGE.
III. ENDORSEMENT PROVISIONS, WITH RESPECT TO THE INSURANCE AFFORDED TO
"ADDITIONAL INSUREDS"
Rev. February 22, 2016
DocuSign Envelope ID: 448F9D83-A76E-4EF1-9A95-3F616E43347D
/1.. PRIMARY-OVERAGE
WITH RESPECT TO CLAIMS ARISING OUT OF THE OPERATIONS OF THE NAMED INSURED,
INSURANCE AS AFFORDED BY THIS POLICY IS PRIMARY AND IS NOT ADDITIONAL TO OR
CONTRIBUTING WITH ANY OTHER INSURANCE CARRIED BY OR FOR THE BENEFIT OF THE
ADDITIONAL INSUREDS.
B. CROSS LIABILITY
THE NAMING OF MORE THAN ONE PERSON, FIRM, OR CORPORATION AS INSUREDS UNDER THE
POLICY SHALL NOT, FOR THAT REASON ALONE, EXTINGUISH ANY RIGHTS OF THE INSURED
AGAINST ANOTHER, BUT THIS ENDORSEMENT, AND THE NAMING OF MULTIPLE INSUREDS,
SHALL NOT INCREASE THE TOTAL LIABILITY OF THE COMPANY UNDER THIS POLICY.
C. OTICE OF CA CELLATlON
I. IF THE POLICY IS CANCELED BEFORE ITS EXPIRATION DATE FOR ANY
REASON OTHER THAN THE NON-PAYMENT OF PREMIUM, THE
CONTRACTOR SHALL PROVIDE CITY AT LEAST A THIRTY (30) DAY
WRITTEN NOTICE BEFORE THE EFFECTIVE DATE OF CANCELLATION.
2. IF THE POLICY IS CANCELED BEFORE ITS EXPIRATION DATE FOR THE NON-
PAYMENT OF PREMIUM, THE CONTRACTOR SHALL PROVIDE CITY AT
LEAST A TEN (10) DAY WRITTEN NOTICE BEFORE THE EFFECTIVE DA TE OF
CANCELLATION.
NOTICES SHALL BE EMAILED TO: lnsuraneeCerts@CityofPaloAlto.org
PURCHASING AND
CONTRACT ADMINISTRATION
CITY OF PALO ALTO
P.O. BOX 10250
PALO AL TO, CA 94303
Rev. February 22, 2016
Attachment B: Bid Result Summary
RFQ 161852: Transportation and Disposal of Ash and Sludge
Bid
Item Bid Schedule Section Description UOM Qty
PSC1 Unit
Price
PSC1 Line
Total
CH2 Unit
Price
CH2 Line
Total
A‐1A: ash hauling & disposal Disposal cost of ash TON 723 $65.00 $46,995.00 $68.00 $49,164.00
A‐2A: ash hauling & disposal Transportation cost of ash: LOAD 53 $1,200.00 $63,600.00 $3,200.00 $169,600.00
A‐3A: ash hauling & disposal Liner installation fee for ash ‐ per load LOAD 53 $50.00 $2,650.00 $57.00 $3,021.00
A‐4A: ash hauling & disposal Bin Rental for ash DAYS 365 $9.00 $3,285.00 $10.00 $3,650.00
A‐5A: ash hauling & disposal CA Non‐RCRA taxes for ash; based on the most current CA BOE schedule TON 723 $23.23 $16,795.29 $0.00 $0.00
A‐6A: ash hauling & disposal Local taxes for ash, as necessary, per ton TON 723 $6.50 $4,699.50 $0.00 $0.00
A‐7A: ash hauling & disposal Surcharges/fees for ash, lump sum LS 1 $0.00 $0.00 $0.00 $0.00
Subtotal $138,024.79 Subtotal $225,435.00
B‐1B: sludge hauling & disposal Disposal cost of sludge TON 150 $22.00 $3,300.00 $71.50 $10,725.00
B‐2B: sludge hauling & disposal Transportation cost for sludge LOAD 12 $600.00 $7,200.00 $710.80 $8,529.60
B‐3B: sludge hauling & disposal Liner installation fee for sludge ‐ per load LOAD 12 $50.00 $600.00 $31.83 $381.96
B‐4B: sludge hauling & disposal Bin Rental DAYS 12 $9.00 $108.00 $10.61 $127.32
B‐5B: sludge hauling & disposal Local taxes, as necessary, per ton TON 150 $0.00 $0.00 $0.00 $0.00
B‐6B: sludge hauling & disposal Surcharges/fees for sludge, lump sum LS 1 $0.00 $0.00 $300.00 $300.00
B‐7B: sludge hauling & disposal Roll‐off bin mobilization during backup sludge hauling service EA 6 $450.00 $2,700.00 $500.00 $3,000.00
B‐8B: sludge hauling & disposal
Onsite truck and truck driver to move empty and full bins in and out of
incinerator building during backup sludge handling service HR 48 $95.00 $4,560.00 $100.79 $4,837.92
Subtotal $18,468.00 Subtotal $27,901.80
Contract Year 1, Total for Bid Schedules A and B Subtotal $156,492.79 Subtotal $253,336.80
Price Increases Estimated price increase ‐ Year 2 (see note 3) % 1 3.00% $4,694.78 3.00% $7,591.10
Price Increases Estimated price increase ‐ Year 3 (see note 3) % 1 3.00% $4,835.63 3.00% $7,818.84
Contract Year 1, Total for Bid Schedules A and B $156,492.79 $253,336.80
Contract Year 2, Total for Bid Schedules A and B $161,187.57 $260,927.90
Contract Year 3, Total for Bid Schedules A and B $166,023.20 $268,746.74
1 PSC Industrial Outsourcing, LP 3y Total $483,703.56 3y Total $783,011.45
2 Clean Harbors Environmental Services, Inc.
3 Clean Harbors Environmental Services, Inc.; 2nd and 3rd year contract price increases on items A‐1, 2, 3, and 4, and B‐1, 2, 3, 4, 7, and 8 only
UOM = unit of measurement; Qty = quantity; LS = lump sum; EA = each; HR = hour
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